2-6-DIMETHYL-4-NITROANILINE

Product Name: 2-6-DIMETHYL-4-NITROANILINE
CAS No.: 16947-63-0
Chemical Name: 2-6-DIMETHYL-4-NITROANILINE
Synonyms: 4-NITRO-2,6-XYLIDINE;2-6-DIMETHYL-4-NITROANILINE;2,6-DIMETHYL-4-NITROANALINE;2,6-Dimethyl-4-nitrobenzenamine;2,6-Dimethyl-4-nitro-phenylamine;Benzenamine, 2,6-dimethyl-4-nitro-;BENZENE DERIVATIVE(2,6-DIMETHYL-4-NITROANILINE)
CBNumber: CB6300100
Molecular Formula: C8H10N2O2
Formula Weight: 166.18
MOL File: 16947-63-0.mol

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2-6-DIMETHYL-4-NITROANILINE Property

Melting point:: 165 °C
Boiling point:: 352.6±37.0 °C(Predicted)
Density: 1.220±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly)
form: Solid
pka: 0.76±0.20(Predicted)
color: Brown

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: D481685
Product name: 2,6-Dimethyl-4-nitroaniline
Packaging: 50mg
Price: $85
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0387920
Product name: 2,6-DIMETHYL-4-NITROANILINE
Purity: 95.00%
Packaging: 5MG
Price: $503.59
Updated: 2021/12/16

Crysdot

Product number: CD12134599
Product name: 2,6-Dimethyl-4-nitroaniline
Purity: 97%
Packaging: 100mg
Price: $95
Updated: 2021/12/16

Crysdot

Product number: CD12134599
Product name: 2,6-Dimethyl-4-nitroaniline
Purity: 97%
Packaging: 250mg
Price: $153
Updated: 2021/12/16

Chemenu

Product number: CM127731
Product name: 2,6-dimethyl-4-nitroaniline
Purity: 95+%
Packaging: 1g
Price: $360
Updated: 2021/12/16

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2-6-DIMETHYL-4-NITROANILINE Chemical Properties,Usage,Production

Synthesis

67083-22-1

16947-63-0

The general procedure for the synthesis of 2,6-dimethyl-4-nitroaniline from N-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide is as follows: N-(2,6-dimethyl-4-nitrophenyl)-4-methylbenzenesulfonamide (3.2 g, 10.0 mmol) was dissolved in 32 mL of concentrated sulfuric acid and the reaction was heated for 1 hr at 50 °C. After completion of the reaction, the mixture was slowly poured into an ice-water mixture. The precipitate precipitated was collected by filtration and washed with cold water. The crude product was purified by recrystallization from ethyl acetate to give 2,6-dimethyl-4-nitroaniline (1.0 g, 53% yield) in yellow crystalline form. Thin layer chromatography (TLC) Rf value was 0.34 (unfolding agent: hexane/ethyl acetate, 5/1, v/v). Melting point: 164-165°C. 1H NMR (DMSO-d6, 400MHz) δ 7.79 (s, 2H), 6.16 (s, 2H), 2.16 (s, 6H). Mass spectrum (ESI) m/z: 166.8 [M+H]+, 188.8 [M+Na]+.

References

[1] Patent: EP3138833, 2017, A1. Location in patent: Paragraph 0040; 0043
[2] European Journal of Organic Chemistry, 2009, # 5, p. 739 - 748
[3] Journal of Medicinal Chemistry, 1983, vol. 26, # 11, p. 1625 - 1630
[4] Heterocycles, 2008, vol. 76, # 2, p. 1313 - 1328
[5] Patent: KR2018/69782, 2018, A. Location in patent: Paragraph 0422; 0424; 0431-0433

2-6-DIMETHYL-4-NITROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-6-DIMETHYL-4-NITROANILINE Suppliers

China 44 France 1 Germany 1 India 6 Switzerland 1 United States 4 Global 57

Adamas Reagent, Ltd.

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Nanjing Vital Chemical Co., Ltd.

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WG reagent

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Amadis Chemical Company Limited

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Aikon International Limited

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View Lastest Price from 2-6-DIMETHYL-4-NITROANILINE manufacturers

Career Henan Chemical Co

Product: 2-6-DIMETHYL-4-NITROANILINE 16947-63-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-14

16947-63-0, 2-6-DIMETHYL-4-NITROANILINERelated Search:

2-(ACETYLAMINO)-3-METHYL-5-NITROBENZOIC ACID Pyrrolo(3,2,1-jk)(1,4)benzodiazepin-4(3H)-one, 6,7-dihydro-9-nitro-1-p henyl- 2,3,5,6-TETRAMETHYL-4-NITROANILINE Disperse Blue 165 7-METHYL-5-NITRO-1H-INDOLE-2,3-DIONE 8-QUINOLINECARBOXYLIC ACID, 1,2,3,4-TETRAHYDRO-6-NITRO- 2-TERT-BUTYL-6-METHYL-4-NITROANILINE 2-AMINO-3-METHYL-5-NITROBENZOIC ACID ASISCHEM W01374 CHEMBRDG-BB 5790744 DINITRODURENE ASISCHEM W03648 2,6-DIISOPROPYL-4-NITROANILINE METHYL 2-(ACETYLAMINO)-3-METHYL-5-NITROBENZOATE 2,6-DITERT-BUTYL-4-NITROANILINE 2-6-DIMETHYL-4-NITROANILINE

4-NITRO-2,6-XYLIDINE

2-6-DIMETHYL-4-NITROANILINE

2,6-Dimethyl-4-nitro-phenylamine

2,6-Dimethyl-4-nitrobenzenamine

2,6-DIMETHYL-4-NITROANALINE

Benzenamine, 2,6-dimethyl-4-nitro-

BENZENE DERIVATIVE(2,6-DIMETHYL-4-NITROANILINE)

16947-63-0