methyl 12-bromododecanoate

Product Name: methyl 12-bromododecanoate
CAS No.: 26825-95-6
Chemical Name: methyl 12-bromododecanoate
Synonyms: methyl 12-bromododecanoate;12-bromo-dodecanoic acid methyl ester;Dodecanoic acid, 12-bromo-, methyl ester
CBNumber: CB63105445
Molecular Formula: C13H25BrO2
Formula Weight: 293.24
MOL File: 26825-95-6.mol

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methyl 12-bromododecanoate Property

storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: liquid
color: Clear, pale lemon

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Safety

HS Code: 2915907098

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

AK Scientific

Product number: 3265CS
Product name: Methyl12-bromododecanoate
Packaging: 250mg
Price: $112
Updated: 2021/12/16

Apolloscientific

Product number: OR471516
Product name: Methyl12-Bromododecanoate
Packaging: 1g
Price: $115
Updated: 2021/12/16

ChemScene

Product number: CS-0129051
Product name: Methyl12-bromododecanoate
Purity: ≥97.0%
Packaging: 1g
Price: $123
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2123-9-38
Product name: Methyl 12-bromododecanoate
Packaging: 1g
Price: $127
Updated: 2021/12/16

ChemScene

Product number: CS-0129051
Product name: Methyl12-bromododecanoate
Purity: ≥97.0%
Packaging: 5g
Price: $477
Updated: 2021/12/16

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methyl 12-bromododecanoate Chemical Properties,Usage,Production

Synthesis

67-56-1

73367-80-3

26825-95-6

Under argon protection, 12-bromododecanoic acid (6) (1.0 g, 3.59 mmol) was dissolved in anhydrous methanol (10 mL) containing concentrated sulfuric acid (200 μL) and the reaction was heated to reflux for 15 hours. After completion of the reaction, methanol was removed by distillation under reduced pressure. The residue was diluted with ethyl acetate (100 mL), washed sequentially with saturated sodium bicarbonate solution (3×20 mL) and brine (2×20 mL), and the organic phase was dried with anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to obtain the crude product. Purification by silica gel column chromatography using petroleum ether/ethyl acetate (97.5:2.5) as eluent afforded the target product methyl 12-bromododecanoate (7) (974 mg, 3.32 mmol, 93% yield) as a colorless oil. The product was analyzed by thin-layer chromatography (TLC, Rf 0.45, petroleum ether/ethyl acetate, 9:1), infrared spectroscopy (IR), nuclear magnetic resonance hydrogen spectroscopy (1H NMR), nuclear magnetic resonance carbon spectroscopy (13C NMR) and high-resolution mass spectrometry (HRMS).

References

[1] Journal of Antibiotics, 1995, vol. 48, # 12, p. 1467 - 1480
[2] Journal of Heterocyclic Chemistry, 2001, vol. 38, # 6, p. 1393 - 1400
[3] Analytical Biochemistry, 2014, vol. 456, # 1, p. 70 - 81
[4] Patent: WO2017/49245, 2017, A2. Location in patent: Paragraph 00539-00540
[5] Patent: WO2017/112865, 2017, A1. Location in patent: Paragraph 00618

methyl 12-bromododecanoate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl 12-bromododecanoate Suppliers

China 31 United Kingdom 1 United States 3 Global 35

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View Lastest Price from methyl 12-bromododecanoate manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: methyl 12-bromododecanoate 26825-95-6
Price: US $2.20-8.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 50kg
Release date: 2025-06-24

PNP Biotech Co. Ltd

Product: methyl 12-bromododecanoate 26825-95-6
Price: US $0.00/kg
Min. Order: 25kg
Purity: 95%
Supply Ability: Inquiry
Release date: 2022-10-13

26825-95-6, methyl 12-bromododecanoateRelated Search:

methyl 12-bromododecanoate

12-bromo-dodecanoic acid methyl ester

Dodecanoic acid, 12-bromo-, methyl ester

26825-95-6

26825-96-5