ChemicalBook > CAS DataBase List > 3-CHLORO-2-METHYLPHENOL
3-CHLORO-2-METHYLPHENOL
- Product Name
- 3-CHLORO-2-METHYLPHENOL
- CAS No.
- 3260-87-5
- Chemical Name
- 3-CHLORO-2-METHYLPHENOL
- Synonyms
- 3-chloro-o-cresol;o-Cresol, 3-chloro-;3-CHLORO-2-METHYLPHENOL;Phenol, 3-chloro-2-methyl-;3-Chloro-2-methylphenol 98%;3-Chloro-2-methylphenol CAS NO.3260-87-5;2-Chloro-6-hydroxytoluene, 3-Chloro-o-cresol
- CBNumber
- CB6372857
- Molecular Formula
- C7H7ClO
- Formula Weight
- 142.58
- MOL File
- 3260-87-5.mol
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3-CHLORO-2-METHYLPHENOL Property
- Melting point:
- 86 °C
- Boiling point:
- 225 °C
- Density
- 1.1104 (rough estimate)
- refractive index
- 1.5449 (estimate)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- powder
- pka
- 9.35±0.10(Predicted)
- color
- Brown
- Sensitive
- Stench
- CAS DataBase Reference
- 3260-87-5(CAS DataBase Reference)
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Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 21/22-41-43-50-38-36
- Safety Statements
- 26-36/37/39-28
- RIDADR
- 3437
- HazardClass
- IRRITANT, IRRITANT-HARMFUL
- HS Code
- 29081990
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- C381458
- Product name
- 3-Chloro-2-methylphenol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FC139545
- Product name
- 3-Chloro-2-methylphenol
- Packaging
- 10g
- Price
- $52
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 2701-5-X3
- Product name
- 3-Chloro-2-methylphenol
- Purity
- 98%
- Packaging
- 5G
- Price
- $116
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 002186
- Product name
- 3-Chloro-2-methylphenol
- Purity
- 98%
- Packaging
- 25g
- Price
- $125
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FC139545
- Product name
- 3-Chloro-2-methylphenol
- Packaging
- 50g
- Price
- $155
- Updated
- 2021/12/16
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3-CHLORO-2-METHYLPHENOL Chemical Properties,Usage,Production
Synthesis
87-60-5
3260-87-5
1. In a 1000 mL three-necked flask equipped with a thermometer, a mechanical stirrer and a dropping funnel, 700 mL of 22% sulfuric acid solution was pre-filled and heated to 70 °C. 2. 8 g of 3-chloro-2-methylaniline was added to the above solution in batches, maintaining the temperature at 70 °C until completely dissolved. 3. The reaction mixture was heated to 90 °C and then cooled to 10-12 °C to form a suspension. 4. the diazotization reaction was carried out by slowly adding 88.4 g of 40% sodium nitrite solution dropwise under stirring, maintaining the temperature at 10-12 °C. 5. the resulting diazonium salt mixture was heated to 90 °C and then slowly added to a mixture containing 200 mL of methyl isobutyl ketone and 2 g of 96% sulfuric acid under vigorous stirring. 6. The reaction was held at 90 °C for about 15 minutes to complete, after which the emulsion was cooled to 70 °C for phase separation. 7. The organic phase was washed with 50 mL of water to remove inorganic impurities. 8. The selectivity of the thermal decomposition step was 99.1% (a/a) by gas chromatography (GC) analysis. 9. The organic phase was purified by distillation to give 66.9 g of 3-chloro-2-methylphenol with a GC purity of 99.2% (a/a). 10. The distillation residue was 2.3 g. The yield of the target product was calculated to be 93.1%.
References
[1] Patent: CN105392764, 2016, A. Location in patent: Paragraph 0026
[2] Patent: WO2007/39563, 2007, A1. Location in patent: Page/Page column 23-24
[3] Patent: US2007/112019, 2007, A1. Location in patent: Page/Page column 12/2
[4] Justus Liebigs Annalen der Chemie, 1906, vol. 350, p. 113
[5] Chemische Berichte, 1904, vol. 37, p. 1021
3-CHLORO-2-METHYLPHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-CHLORO-2-METHYLPHENOL manufacturers
Shaanxi Dideu Medichem Co. Ltd
- Product
- 3-CHLORO-2-METHYLPHENOL 3260-87-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 20T
- Release date
- 2024-07-11
Career Henan Chemical Co
- Product
- 3-CHLORO-2-METHYLPHENOL 3260-87-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-20
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