ChemicalBook > CAS DataBase List > ETHYL ADENINE-9-ACETATE

ETHYL ADENINE-9-ACETATE

Product Name: ETHYL ADENINE-9-ACETATE
CAS No.: 25477-96-7
Chemical Name: ETHYL ADENINE-9-ACETATE
Synonyms: ETHYL ADENINE-9-ACETATE;ETHYL ADENINE-9-ACETATE 97%;Adenine acetic acid ethyl ester;ethyl 2-(9H-adenin-9-yl)acetate;Ethyl2-(6-amino-9H-purin-9-yl)acetate;6-Amino-9H-purine-9-acetic acid ethyl ester;9H-Purine-9-acetic acid, 6-amino-, ethyl ester;(6-Amino-9H-purine-9-yl)acetic acid ethyl ester;2-(6-Amino-9H-purin-9-yl)acetic acid ethyl ester
CBNumber: CB6375621
Molecular Formula: C9H11N5O2
Formula Weight: 221.22
MOL File: 25477-96-7.mol

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ETHYL ADENINE-9-ACETATE Property

Melting point:: 224-228 °C (dec.)(lit.)
Boiling point:: 443.1±55.0 °C(Predicted)
Density: 1.52±0.1 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 3.78±0.10(Predicted)
Appearance: Off-white to pink Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B433858
Product name: EthylAdenine-9-acetate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

ChemScene

Product number: CS-0037933
Product name: Ethyl2-(6-amino-9H-purin-9-yl)acetate
Packaging: 1g
Price: $71
Updated: 2021/12/16

ChemScene

Product number: CS-0037933
Product name: Ethyl2-(6-amino-9H-purin-9-yl)acetate
Packaging: 5g
Price: $291
Updated: 2021/12/16

AK Scientific

Product number: J50080
Product name: Ethyladenine-9-acetate
Packaging: 10g
Price: $312
Updated: 2021/12/16

Ambeed

Product number: A174863
Product name: Ethyladenine-9-acetate
Purity: 95%
Packaging: 250mg
Price: $25
Updated: 2021/12/16

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ETHYL ADENINE-9-ACETATE Chemical Properties,Usage,Production

Synthesis

105-36-2

66224-66-6

25477-96-7

Example 26 Synthesis of ethyl 9-carboxymethyladenine: Adenine (10 g, 74 mmol) and potassium carbonate (10.29 g, 74 mmol) were suspended in N,N-dimethylformamide (DMF) followed by the addition of ethyl bromoacetate (8.24 mL, 74 mmol). The reaction mixture was stirred at room temperature and under nitrogen protection for 2.5 h. After completion of the reaction, it was filtered. The solid residue was washed three times with DMF (10 mL). All filtrates were combined and the solvent was removed by distillation under reduced pressure to give a yellow-orange solid. To this solid, water (200 mL) was added and the pH was adjusted to 6 with 4 N hydrochloric acid. after stirring for 10 min at 0 °C, the precipitate was collected, washed with water and purified by recrystallization in 96% ethanol (150 mL). Isolation by filtration gave N-ethyl acetate adenopyrimidine and the product was washed thoroughly with ether. The final yield was 3.4 g (20% yield) with a melting point of 215.5-220°C. Elemental analysis results (C9H11N5O2 calculated/measured values): C: 48.65/48.86; H: 4.91/5.01; N: 31.42/31.66. Nuclear magnetic resonance hydrogen spectrum (250 MHz, DMSO-d6): δ 7.25 (broad single peak, 2H, NH), 5.06 (single peak, 2H, NCH2), 4.17 (quadruple peak , 2H, J=7.11Hz, OCH2), 1.21 (triple peak, 3H, J=7.13Hz, CH3). NMR carbon spectrum showed major peaks located at 152.70, 141.30, 61.41, 43.97 and 14.07 ppm. fast atom bombardment mass spectrometry (FAB-MS) showed molecular ion peak m/z 222 (MH+). IR spectra (cm-1, intensity): 3855 (54.3), 3274 (10.4), 3246 (14.0), 3117 (5.3), 2989 (22.3), 2940 (33.9), 2876 (43.4), 2753 (49.0), 2346 (56.1), 2106 (57.1), 1899 ( 55.7), 1762 (14.2), 1742 (14.2), 1671 (1.8), 1644 (10.9), 1606 (0.6), 1582 (7.1), 1522 (43.8), 1477 (7.2), 1445 (35.8), 1422 (8.6).

References

[1] Journal of Organic Chemistry, 1994, vol. 59, # 19, p. 5767 - 5773
[2] Tetrahedron, 2005, vol. 61, # 34, p. 8295 - 8305
[3] Journal of the Chemical Society, Perkin Transactions 1, 2000, # 1, p. 19 - 26
[4] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 7, p. 2300 - 2313
[5] Dalton Transactions, 2012, vol. 41, # 33, p. 10043 - 10051

ETHYL ADENINE-9-ACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from ETHYL ADENINE-9-ACETATE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: ETHYL ADENINE-9-ACETATE 25477-96-7
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-11

Zhuozhou Wenxi import and Export Co., Ltd

Product: ETHYL ADENINE-9-ACETATE 25477-96-7
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

25477-96-7, ETHYL ADENINE-9-ACETATERelated Search:

Adenine ETHYL ADENINE-9-ACETATE

ETHYL ADENINE-9-ACETATE

ETHYL ADENINE-9-ACETATE 97%

Adenine acetic acid ethyl ester

(6-Amino-9H-purine-9-yl)acetic acid ethyl ester

2-(6-Amino-9H-purin-9-yl)acetic acid ethyl ester

6-Amino-9H-purine-9-acetic acid ethyl ester

Ethyl2-(6-amino-9H-purin-9-yl)acetate

9H-Purine-9-acetic acid, 6-amino-, ethyl ester

ethyl 2-(9H-adenin-9-yl)acetate

25477-96-7

ACETATE