ChemicalBook > CAS DataBase List > CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER

CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER

Application

Product Name: CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER
CAS No.: 62638-06-6
Chemical Name: CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER
Synonyms: diMethyl cyclohexane-1,3-dicarboxylate;Dimethyl 1,3-cyclohexane dicarboxylate;Dimethyl cyclohexane-1,3-dixarboxylate;1,3-dimethyl cyclohexane-1,3-dicarboxylate;CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER;1,3-Cyclohexanedicarboxylic acid, 1,3-dimethyl ester
CBNumber: CB6403544
Molecular Formula: C10H16O4
Formula Weight: 200.23
MOL File: 62638-06-6.mol

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CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Property

Boiling point:: 258.1±15.0℃ (760 Torr)
Density: 1.102±0.06 g/cm3 (20 ºC 760 Torr)
refractive index: 1.4592 (589.3 nm 18℃)
Flash point:: 120.7±18.8℃
storage temp.: Sealed in dry,Room Temperature
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D482570
Product name: dimethylcyclohexane-1,3-dicarboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: D482570
Product name: dimethylcyclohexane-1,3-dicarboxylate
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD142268
Product name: Dimethyl cyclohexane-1,3-dicarboxylate
Packaging: 50mg
Price: $67
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD142268
Product name: Dimethyl cyclohexane-1,3-dicarboxylate
Packaging: 100mg
Price: $116
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD142268
Product name: Dimethyl cyclohexane-1,3-dicarboxylate
Packaging: 250mg
Price: $230
Updated: 2021/12/16

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CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Chemical Properties,Usage,Production

Application

Dimethyl 1,3-cyclohexanoate can be used as a pharmaceutical synthesis intermediate and an organic synthesis intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical synthesis processes.

Synthesis

67-56-1

3971-31-1

62638-06-6

1. cyclohexane-1,3-dicarboxylic acid (10.32 g, 60 mmol) was dissolved in methanol (130 mL). 2. Concentrated sulfuric acid (2.5 mL) was added as a catalyst and the reaction mixture was heated to reflux and stirred for 16 hours. 3. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure to remove most of the methanol. 4. The residue was adjusted to pH 7 with saturated aqueous sodium bicarbonate. 5. The aqueous phase was extracted with ethyl acetate (200 mL × 3) and the organic layers were combined. 6. 6. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give dimethyl 1,3-cyclohexanedioate as a colorless oil (12 g, 100% yield). 7. The product was analyzed by 1H NMR. 7. The product was characterized by 1H NMR (400 MHz, DMSO-d6) and mass spectrometry (ESI): 1H NMR δ 3.61 (s, 6H), 2.69-1.13 (m, 10H); MS (ESI) m/e [M + 1] 201.1.

References

[1] Patent: WO2016/161960, 2016, A1. Location in patent: Paragraph 0542
[2] Acta Crystallographica Section C: Crystal Structure Communications, 2013, vol. 69, # 7, p. 727 - 729
[3] Patent: WO2012/88365, 2012, A1. Location in patent: Page/Page column 24
[4] Patent: WO2013/40535, 2013, A2. Location in patent: Page/Page column 23
[5] Patent: WO2016/106623, 2016, A1. Location in patent: Page/Page column 122

CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER manufacturers

Shanghai Yongzeng Technology Co.,Ltd

Product: Dimethyl cyclohexane-1,3-dixarboxylate 62638-06-6
Price: US $0.00/gm
Min. Order: 100gm
Purity: 97%
Supply Ability: 100kgs
Release date: 2024-09-11

62638-06-6, CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTERRelated Search:

Bicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acid dianhydride Dimethyl 1,3-adamantanedicarboxylate Trimethyl cis,cis-1,3,5-cyclohexanetricarboxylate DIETHYL 2-(BENZO[D][1,3]DIOXOL-5-YL)-4-HYDROXY-4-METHYL-6-OXOCYCLOHEXANE-1,3-DICARBOXYLATE DIETHYL 2-(4-ETHOXYPHENYL)-4-HYDROXY-4-METHYL-6-OXOCYCLOHEXANE-1,3-DICARBOXYLATE TetramethylBicyclo[2.2.2]-7-octene-2,3,5,6-tetracarboxylate AKOS BB-2935 TRIMETHYL CIS,CIS-1,3,5-TRIPROPYL-1,3,5-CYCLOHEXANETRICARBOXYLATE AKOS BC-1751 DIMETHYL 2-HYDROXYCYCLOHEXANE-1,3-DICARBOXYLATE AKOS B024699 AKOS B024698 1,14-DIMETHYL-4,10-DIOXATETRACYCLO[5.5.2.0(2,6).0(8,12)]TETRADEC-13-ENE-3,5,9,11-TETRAONE AKOS B024701 AKOS BB-2936 ETHYL 3,5-DIOXO-4-OXATRICYCLO[5.2.2.0(2,6)]UNDEC-8-ENE-1-CARBOXYLATE ETHYL 3,5-DIOXO-4-OXATRICYCLO[5.2.2.0(2,6)]UNDECANE-1-CARBOXYLATE AKOS BC-1672

Dimethyl 1,3-cyclohexane dicarboxylate

CYCLOHEXANE-1,3-DICARBOXYLIC ACID DIMETHYL ESTER

diMethyl cyclohexane-1,3-dicarboxylate

1,3-dimethyl cyclohexane-1,3-dicarboxylate

1,3-Cyclohexanedicarboxylic acid, 1,3-dimethyl ester

Dimethyl cyclohexane-1,3-dixarboxylate

62638-06-6