4-ISOPROPYL-2-NITROANILINE
- Product Name
- 4-ISOPROPYL-2-NITROANILINE
- CAS No.
- 63649-64-9
- Chemical Name
- 4-ISOPROPYL-2-NITROANILINE
- Synonyms
- BUTTPARK 89\07-12;4-ISOPROPYL-2-NITROANILINE;2-nitro-4-(propan-2-yl)aniline;BENZENAMINE, 4-(1-METHYLETHYL)-2-NITRO-;2-Nitro-4-(prop-2-yl)aniline, 4-Amino-3-nitrocumene
- CBNumber
- CB6447645
- Molecular Formula
- C9H12N2O2
- Formula Weight
- 180.2
- MOL File
- 63649-64-9.mol
4-ISOPROPYL-2-NITROANILINE Property
- Melting point:
- 36-39
- Boiling point:
- 142-144/0.4mm
- Density
- 1.172±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 0.40±0.10(Predicted)
- Appearance
- Yellow to orange Solid
Safety
- Hazard Codes
- T
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 26-36/37/39
- Hazard Note
- Toxic
- HS Code
- 2921420090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I872803
- Product name
- 4-Isopropyl-2-nitroaniline
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- I872803
- Product name
- 4-Isopropyl-2-nitroaniline
- Packaging
- 500mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- Y5060
- Product name
- 4-Isopropyl-2-nitroaniline
- Packaging
- 5g
- Price
- $439
- Updated
- 2021/12/16
- Product number
- 4755-1-X1
- Product name
- 4-Isopropyl-2-nitroaniline
- Packaging
- 500mg
- Price
- $128
- Updated
- 2021/12/16
- Product number
- 4755-1-X1
- Product name
- 4-Isopropyl-2-nitroaniline
- Packaging
- 1g
- Price
- $199
- Updated
- 2021/12/16
4-ISOPROPYL-2-NITROANILINE Chemical Properties,Usage,Production
Synthesis
1338684-26-6
63649-64-9
The general procedure for the synthesis of 4-isopropyl-2-nitroaniline from 2,2,2-trifluoro-N-(2-nitro-4-isopropylphenyl)acetamide was as follows: to a stirring solution of 2,2,2-trifluoro-N-(4-isopropyl-2-nitrophenyl)acetamide (2.1 g, 7.6 mmol) in methanol (40 mL) was added sequentially water (20 mL) and potassium carbonate ( 0.5 g, 4 mmol). The reaction mixture was stirred at room temperature for 18 h, followed by partition extraction with ethyl acetate (50 mL) and saturated saline (50 mL). After separation of the organic layer, the aqueous layer was then extracted with ethyl acetate (3 x 25 mL). All organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (silica gel 230-400 mesh, 150 g, eluting sequentially with 20% and 30% ethyl acetate/hexane solvent mixture) to afford 4-isopropyl-2-nitroaniline 1.18 g (61% yield) as an orange oil. Its NMR hydrogen spectrum (CDCl3) data were as follows: δ 1.23 (6H, d), 2.85 (1H, m), 6.77 (1H, d), 7.28 (1H, dd), 7.96 (1H, d). Mass spectrometry (ESI+) showed the molecular ion peak m/z 181.2 ([M+H]+). The HPLC (Method D) retention time was 3.97 min.
References
[1] Patent: WO2011/126567, 2011, A1. Location in patent: Page/Page column 187
4-ISOPROPYL-2-NITROANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-ISOPROPYL-2-NITROANILINE manufacturers
- Product
- 2-nitro-4-propan-2-ylaniline 63649-64-9
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-10
- Product
- 4-ISOPROPYL-2-NITROANILINE 63649-64-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-08