ChemicalBook > CAS DataBase List > Methyl 5-thiazolecarboxylate

Methyl 5-thiazolecarboxylate

Product Name
Methyl 5-thiazolecarboxylate
CAS No.
14527-44-7
Chemical Name
Methyl 5-thiazolecarboxylate
Synonyms
NSC 321257;RARECHEM AL BF 1261;Methyl 5-thiazolecar;5-thiazole carboxylate.;METHYL 5-THIAZOLECARBOXYLATE;METHYL THIAZOLE-5-CARBOXYLATE;5-(Methoxycarbonyl)-1,3-thiazole;methyl 1,3-thiazole-5-carboxylate;Methyl 1,3-thiazole-5-carboxylate 98%;Thiazole-5-carboxylic acid methyl ester
CBNumber
CB6481766
Molecular Formula
C5H5NO2S
Formula Weight
143.16
MOL File
14527-44-7.mol
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Methyl 5-thiazolecarboxylate Property

Melting point:
68-69°C
Boiling point:
87-90°C (10 mmHg)
Density 
1.45
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
0.80±0.10(Predicted)
Appearance
Off-white to light yellow Solid
CAS DataBase Reference
14527-44-7(CAS DataBase Reference)
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Safety

Hazard Codes 
Xn
Risk Statements 
36/37/38-22
Safety Statements 
26-36/37/39
Hazard Note 
Harmful
HS Code 
2934100090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
M331478
Product name
MethylThiazole-5-carboxylate
Packaging
10mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
8H70-1-V8
Product name
Methyl 1,3-thiazole-5-carboxylate
Packaging
250mg
Price
$35
Updated
2021/12/16
AK Scientific
Product number
C222
Product name
Methylthiazole-5-carboxylate
Packaging
1g
Price
$40
Updated
2021/12/16
SynQuest Laboratories
Product number
8H70-1-V8
Product name
Methyl 1,3-thiazole-5-carboxylate
Packaging
1g
Price
$105
Updated
2021/12/16
ChemScene
Product number
CS-M1604
Product name
5-Thiazolecarboxylicacid,methylester
Packaging
5g
Price
$129
Updated
2021/12/16
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Methyl 5-thiazolecarboxylate Chemical Properties,Usage,Production

Synthesis

6633-61-0

14527-44-7

The general procedure for the synthesis of methyl 5-thiazolecarboxylate from methyl 2-aminothiazole-5-carboxylate was as follows: a mixture of 2.25 g of isoamyl nitrite with 10 mL of dioxane was stirred at 80 °C under nitrogen protection. Subsequently, a 20 mL dioxane solution containing 1.23 g of methyl 2-aminothiazole-5-carboxylate (g-3) was slowly added dropwise. After the dropwise addition was completed, the reaction mixture was refluxed for 2 hours. After the reaction was completed, it was cooled to room temperature and diluted by adding 30 mL of ethyl acetate. The organic phase was washed with saturated saline, dried over anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography to give 0.54 g (48% yield) of the target product methyl 5-thiazolecarboxylate (g-4).

References

[1] Patent: WO2003/97616, 2003, A1. Location in patent: Page/Page column 26

Methyl 5-thiazolecarboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 5-thiazolecarboxylate manufacturers

Career Henan Chemical Co
Product
Methyl 5-thiazolecarboxylate 14527-44-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2019-12-26

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  • Methyl 1,3-thiazole-5-carboxylate 98%
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