ChemicalBook > CAS DataBase List > 6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&

6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&

Product Name
6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&
CAS No.
36684-65-8
Chemical Name
6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&
Synonyms
NSC 298291;1,2,3,4-Tetrahydro-6-chlorocarbazole;6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&;6-Chloro-1,2,3,4-tetrahydrocarbazole >1H-Carbazole, 6-chloro-2,3,4,9-tetrahydro-;6-CHLORO-1,2,3,4-TETRAHYDROCARBAZOLE, 98 %
CBNumber
CB6504474
Molecular Formula
C12H12ClN
Formula Weight
205.68
MOL File
36684-65-8.mol
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6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& Property

Melting point:
145-148 °C (lit.)
Boiling point:
358.8±37.0 °C(Predicted)
Density 
1.280
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
slightly sol. in Methanol
form 
powder to crystal
pka
16.93±0.20(Predicted)
color 
White to Light yellow
λmax
292nm(ethylene glycol)(lit.)
InChI
InChI=1S/C12H12ClN/c13-8-5-6-12-10(7-8)9-3-1-2-4-11(9)14-12/h5-7,14H,1-4H2
InChIKey
CNQQPGJXOHSTQR-UHFFFAOYSA-N
SMILES
N1C2=C(C=C(Cl)C=C2)C2=C1CCCC2
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HS Code 
2933.99.8290
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
517577
Product name
6-Chloro-1,2,3,4-tetrahydrocarbazole
Purity
98%
Packaging
1g
Price
$72
Updated
2023/06/20
TCI Chemical
Product number
C2857
Product name
6-Chloro-1,2,3,4-tetrahydrocarbazole
Purity
>98.0%(GC)
Packaging
1g
Price
$81
Updated
2024/03/01
TCI Chemical
Product number
C2857
Product name
6-Chloro-1,2,3,4-tetrahydrocarbazole
Purity
>98.0%(GC)
Packaging
5g
Price
$241
Updated
2024/03/01
TRC
Product number
C433413
Product name
6-Chloro-2,3,4,9-tetrahydro-1H-carbazole
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
4659AB
Product name
6-Chloro-2,3,4,9-tetrahydro-1H-carbazole
Packaging
5g
Price
$201
Updated
2021/12/16
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6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& Chemical Properties,Usage,Production

Synthesis

1073-70-7

108-94-1

36684-65-8

GENERAL METHODS: Cyclohexanone (0.91 g, 10.0 mmol) was mixed with bis(trifluoromethanesulfonyl)imide salt ([(HSO3-p)2im][CF3SO3]) (0.5 mmol) in deionized water (15 mL), followed by the addition of p-chlorophenylhydrazine hydrochloride (1.44 g, 10.0 mmol). The reaction mixture was placed in a microwave reactor and stirred at 100 °C for about 15 min, and the reaction process was monitored by gas chromatography-mass spectrometry (GC-MS). After completion of the reaction, the mixture was cooled to room temperature and the precipitate was collected by filtration to afford 6-chloro-1,2,3,4-tetrahydrocarbazole. The mixed system of [(HSO3-p)2im][CF3SO3]/H2O used in the reaction can be directly recycled for subsequent reactions.

References

[1] Journal of Fluorine Chemistry, 2012, vol. 144, p. 45 - 50,6
[2] Tetrahedron Letters, 2018, vol. 59, # 22, p. 2145 - 2149
[3] Heterocyclic Communications, 2003, vol. 9, # 1, p. 9 - 12
[4] Organic and Biomolecular Chemistry, 2016, vol. 14, # 41, p. 9868 - 9873
[5] Patent: CN105968039, 2016, A. Location in patent: Paragraph 0049-0051

6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& Preparation Products And Raw materials

Raw materials

Preparation Products

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6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& Suppliers

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View Lastest Price from 6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& manufacturers

Career Henan Chemical Co
Product
6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9 36684-65-8
Price
US $0.01/KG
Min. Order
1KG
Purity
98%; 99%
Supply Ability
500g;1kg； 25kg
Release date
2020-01-09

36684-65-8, 6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&Related Search:

6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9& 1,2,3,4-Tetrahydrocarbazole 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE-1-CARBOXYLIC ACID 3-CHLORO-6,7,8,9-TETRAHYDRO-5H-CARBAZOLE-2-CARBOXYLIC ACID 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE-1-CARBOXAMIDE ETHYL 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE-1-CARBOXYLATE 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE 3-CHLORO-6,7,8,9-TETRAHYDRO-5H-CARBAZOLE-4-CARBOXYLIC ACID 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-OL 1,10-Trimethylene-2-propyl-8-chloro-1,2,3,4-tetrahydropyrazino(1,2-a)i ndole hydrochloride 1,10-Trimethylene-2-butyl-8-chloro-1,2,3,4-tetrahydropyrazino(1,2-a)in dole hydrochloride AURORA KA-6354 6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE-1-CARBONITRILE 6-CHLORO-N'-HYDROXY-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE-1-CARBOXIMIDAMIDE AURORA KA-8108 AURORA KA-3292 AURORA KA-8102 6-CHLORO-1-(1H-TETRAZOL-5-YL)-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE

  • 6-CHLORO-1 2 3 4-TETRAHYDROCARBAZOLE 9&
  • 1,2,3,4-Tetrahydro-6-chlorocarbazole
  • NSC 298291
  • 6-CHLORO-1,2,3,4-TETRAHYDROCARBAZOLE, 98 %
  • 6-Chloro-1,2,3,4-tetrahydrocarbazole &gt
  • 1H-Carbazole, 6-chloro-2,3,4,9-tetrahydro-
  • 36684-65-8
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