2-(BENZYLAMINO)ACETONITRILE
- Product Name
- 2-(BENZYLAMINO)ACETONITRILE
- CAS No.
- 3010-05-7
- Chemical Name
- 2-(BENZYLAMINO)ACETONITRILE
- Synonyms
- UKRORGSYN-BB BBV-144762;2-(BENZYLAMINO)ACETONITRILE;2-(BENZYLAMINO)ACETONITRILE-2;2-[(Phenylmethyl)amino]-acetonitrile;Acetonitrile, 2-[(phenylMethyl)aMino]-
- CBNumber
- CB6594370
- Molecular Formula
- C9H10N2
- Formula Weight
- 146.19
- MOL File
- 3010-05-7.mol
2-(BENZYLAMINO)ACETONITRILE Property
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- Appearance
- Light yellow to yellow Liquid
Safety
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H314Causes severe skin burns and eye damage
H332Harmful if inhaled
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 119852
- Product name
- 2-(Benzylamino)acetonitrile
- Purity
- 95+%
- Packaging
- 1g
- Price
- $504
- Updated
- 2021/12/16
- Product number
- CHM0106927
- Product name
- 2-(BENZYLAMINO)ACETONITRILE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $852.55
- Updated
- 2021/12/16
- Product number
- CHM0106927
- Product name
- 2-(BENZYLAMINO)ACETONITRILE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1227.82
- Updated
- 2021/12/16
- Product number
- CHM0106927
- Product name
- 2-(BENZYLAMINO)ACETONITRILE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1548.26
- Updated
- 2021/12/16
- Product number
- 3124AB
- Product name
- 2-(Benzylamino)acetonitrile
- Packaging
- 250mg
- Price
- $169
- Updated
- 2021/12/16
2-(BENZYLAMINO)ACETONITRILE Chemical Properties,Usage,Production
Synthesis
107-14-2
100-46-9
3010-05-7
To a suspension of benzylamine (1.0 mL, 9.2 mmol) and potassium carbonate (3.0 g, 22.0 mmol) in acetonitrile (25.4 mL) was added dropwise chloroacetonitrile (0.90 mL, 14.0 mmol). The reaction mixture was stirred at 60 °C for 16 hours. Upon completion of the reaction, the mixture was allowed to cool to room temperature and the excess solvent was subsequently removed under reduced pressure. The residue was diluted with dichloromethane, washed sequentially with saturated sodium bicarbonate solution and brine, the organic phase was dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography to afford 2-(benzylamino)acetonitrile (1.2 g, 90% yield).LCMS (formic acid as additive): m/z 147.2 ([M+H]+).
References
[1] Patent: WO2013/14448, 2013, A1. Location in patent: Page/Page column 103; 104
[2] Tetrahedron, 1998, vol. 54, # 49, p. 14859 - 14868
[3] Synthesis, 2000, # 9, p. 1299 - 1304
[4] Organic Syntheses, 2003, vol. 80, p. 207 - 218
[5] Patent: WO2015/108861, 2015, A1. Location in patent: Paragraph 00425
2-(BENZYLAMINO)ACETONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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