ChemicalBook > CAS DataBase List > 3-(2-BROMO-PHENYL)-PROPAN-1-OL

3-(2-BROMO-PHENYL)-PROPAN-1-OL

Product Name
3-(2-BROMO-PHENYL)-PROPAN-1-OL
CAS No.
52221-92-8
Chemical Name
3-(2-BROMO-PHENYL)-PROPAN-1-OL
Synonyms
Benzenepropanol, 2-bromo-;3-(2-BroMophenyl)-1-propanol;3-(2-BROMO-PHENYL)-PROPAN-1-OL;3-(2-Bromophenyl)propan-1-ol,97%;3-(2-Bromophenyl)-1-propanol,98%
CBNumber
CB6839394
Molecular Formula
C9H11BrO
Formula Weight
215.09
MOL File
52221-92-8.mol
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3-(2-BROMO-PHENYL)-PROPAN-1-OL Property

Boiling point:
106-108 °C(Press: 0.5 Torr)
Density 
1.410±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
15.00±0.10(Predicted)
form 
Liquid
color 
Colorless
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
B698530
Product name
3-(2-Bromo-phenyl)-propan-1-ol
Packaging
1g
Price
$75
Updated
2021/12/16
ChemScene
Product number
CS-W021756
Product name
3-(2-Bromo-phenyl)-propan-1-ol
Purity
97.24%
Packaging
5g
Price
$76
Updated
2021/12/16
AK Scientific
Product number
J55088
Product name
3-(2-Bromo-phenyl)-propan-1-ol
Packaging
5g
Price
$80
Updated
2021/12/16
AK Scientific
Product number
7351AB
Product name
3-(2-Bromo-phenyl)-propan-1-ol
Packaging
5g
Price
$107
Updated
2021/12/16
ChemScene
Product number
CS-W021756
Product name
3-(2-Bromo-phenyl)-propan-1-ol
Purity
97.24%
Packaging
10g
Price
$124
Updated
2021/12/16
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3-(2-BROMO-PHENYL)-PROPAN-1-OL Chemical Properties,Usage,Production

Synthesis

15115-58-9

52221-92-8

General procedure for the synthesis of 2-bromophenylpropanol from 3-(2-bromophenyl)propionic acid: to an anhydrous tetrahydrofuran (5.0 mL) solution of 3-(2-bromophenyl)propionic acid (1.0 g, 4.4 mmol) was slowly added a tetrahydrofuran solution of the borane-tetrahydrofuran complex (1.0 M, 7.0 mL, 7.0 mmol) at 0 °C, and the addition time was controlled at 15 The addition time was controlled to be more than 15 minutes. After addition, the reaction mixture was continued to be stirred at 0 °C for 1 hour. Upon completion of the reaction, the residual borane was quenched by careful addition of water (1 mL) and the solvent was subsequently removed under reduced pressure. The resulting residue was dissolved in ether (20 mL), the organic layer was washed sequentially with water (20 mL) and brine (20 mL), dried over anhydrous sodium sulfate, filtered, and the filtrate was concentrated under reduced pressure to afford 3-(2-bromophenyl)propan-1-ol as a colorless oil (938 mg, quantitative yield). The product did not require further purification and could be used directly in the subsequent reaction.

References

[1] Patent: US2016/95858, 2016, A1. Location in patent: Paragraph 4462; 4463
[2] Journal of Organic Chemistry, 1989, vol. 54, # 23, p. 5574 - 5580
[3] Patent: WO2010/45212, 2010, A2. Location in patent: Page/Page column 222-223
[4] Patent: US2013/184313, 2013, A1. Location in patent: Paragraph 1274; 1275
[5] Angewandte Chemie - International Edition, 2018, vol. 57, # 18, p. 5124 - 5128

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Raw materials

Preparation Products

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View Lastest Price from 3-(2-BROMO-PHENYL)-PROPAN-1-OL manufacturers

Career Henan Chemical Co
Product
3-(2-BROMO-PHENYL)-PROPAN-1-OL 52221-92-8
Price
US $2.00/KG
Min. Order
1g
Purity
98%min
Supply Ability
ask
Release date
2020-01-08

52221-92-8, 3-(2-BROMO-PHENYL)-PROPAN-1-OLRelated Search:

(R)-N-BOC-2-Bromophenylalanine (S)-N-BOC-2-Bromophenylalanine FMOC-D-2-BROMOPHENYLALANINE FMOC-L-2-BROMOPHENYLALANINE 3-(2-Bromophenyl)propionic acid 3-(2-BROMO-4-CHLOROPHENYL)-BETA-ALANINE Benzenepropanoic acid, 2-bromo-4,5-dimethoxy- (9CI) 3-(2-Bromo-phenyl)-3-tert-butoxycarboxycarbonylamino-propionic acid N-FMOC-3-AMINO-3-(2-BROMO-PHENYL)-PROPIONIC ACID 2-AMINO-3-METHYLQUINOLINE HYDROCHLORIDE ETHYL 3-AMINO-3-(2-BROMO-4-METHYLPHENYL)PROPANOATE HYDROCHLORIDE ETHYL 3-AMINO-3-(2-BROMO-4-FLUOROPHENYL)PROPANOATE HYDROCHLORIDE 3-(2-BROMOPHENYL)-3-(1-OXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPANOIC ACID RARECHEM DK HC T304 AKOS BBS-00001989 4-(2-BROMOPHENYL)-1,4-DIHYDRO-2,6-DIMETHYL-3,5-PYRIDINEDICARBOXYLIC ACID DIETHYL ESTER 3-AMINO-3-(2-BROMO-4-METHYL-PHENYL)-PROPIONIC ACID AKOS BBS-00001986

  • 3-(2-BROMO-PHENYL)-PROPAN-1-OL
  • 3-(2-BroMophenyl)-1-propanol
  • Benzenepropanol, 2-bromo-
  • 3-(2-Bromophenyl)-1-propanol,98%
  • 3-(2-Bromophenyl)propan-1-ol,97%
  • 52221-92-8