1,2-Dinitro-4-bromobenzene
- Product Name
- 1,2-Dinitro-4-bromobenzene
- CAS No.
- 610-38-8
- Chemical Name
- 1,2-Dinitro-4-bromobenzene
- Synonyms
- 3,4-Dinitrobromobenzene;1,2-Dinitro-4-bromobenzene;1-Bromo-3,4-dinitrobenzene;Benzene, 4-bromo-1,2-dinitro-
- CBNumber
- CB6851561
- Molecular Formula
- C6H3BrN2O4
- Formula Weight
- 247
- MOL File
- 610-38-8.mol
1,2-Dinitro-4-bromobenzene Property
- Melting point:
- 59-59.5 °C
- Boiling point:
- 353.6±22.0 °C(Predicted)
- Density
- 1.910±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FB140096
- Product name
- 4-Bromo-1,2-dinitrobenzene
- Packaging
- 500mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- FB140096
- Product name
- 4-Bromo-1,2-dinitrobenzene
- Packaging
- 1g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- FB140096
- Product name
- 4-Bromo-1,2-dinitrobenzene
- Packaging
- 5G
- Price
- $485
- Updated
- 2021/12/16
- Product number
- HCH0123113
- Product name
- 1,2-DINITRO-4-BROMOBENZENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $499.87
- Updated
- 2021/12/16
- Product number
- FB140096
- Product name
- 4-Bromo-1,2-dinitrobenzene
- Packaging
- 10g
- Price
- $843.8
- Updated
- 2021/12/16
1,2-Dinitro-4-bromobenzene Chemical Properties,Usage,Production
Synthesis
875-51-4
610-38-8
General procedure for the synthesis of 4-bromo-1,2-dinitrobenzene from 4-bromo-2-nitroaniline: 4-bromo-2-nitroaniline (4.96 g, 22.96 mmol) was added to cold trifluoroacetic acid (25 mL) at 0 °C. After stirring for 10 min, 33% hydrogen peroxide solution (13.75 mL, 133 mmol) was slowly added and the reaction mixture was stirred at room temperature for 0.5 h. Subsequently, it was warmed up to 50 °C and continued to be stirred for 2 h. Upon completion of the reaction, the mixture was poured into ice water, the precipitated solid was collected by filtration and washed with cold water to afford the target compound 4-bromo-1,2-dinitrobenzene. Yield: 76%, yellow solid.1H NMR (500 MHz, CDCl3) δ 7.85-7.92 (m, 2H, H-5, H-6), 8.04 (br.s, 1H, H-3).13C NMR (125.7 MHz, CDCl3) δ 126.39 (C-2), 127.91 (C-3), 128.09 (C- 4), 136.29 (C-5), 141.26 (C-1), 143.42 (C-2). Elemental analysis (C6H3BrN2O4) Calculated values: C, 29.18; H, 1.22; N, 11.34%. Measured values: C, 29.12; H, 1.26; N, 11.26%.
References
[1] Journal of Enzyme Inhibition and Medicinal Chemistry, 2014, vol. 29, # 2, p. 281 - 291
[2] Patent: US8901304, 2014, B1. Location in patent: Page/Page column 12
1,2-Dinitro-4-bromobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,2-Dinitro-4-bromobenzene manufacturers
- Product
- 1,2-Dinitro-4-bromobenzene 610-38-8
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 2000tons
- Release date
- 2025-08-13