Ethyl 2-(2-bromophenyl)acetate
Uses- Product Name
- Ethyl 2-(2-bromophenyl)acetate
- CAS No.
- 2178-24-7
- Chemical Name
- Ethyl 2-(2-bromophenyl)acetate
- Synonyms
- Ivankasse impurity 25;Ethyl 2-bromobenzeneacetate;Ethyl 2-(2-bromophenyl)ethanoate;2-Bromophenylacetic acid ethyl ester;Ethyl (2-bromophenyl)acetate - [E72192];(2-Brom-phenyl)-essigsaeure-aethylester;Benzeneacetic acid, 2-broMo-, ethyl ester
- CBNumber
- CB6853343
- Molecular Formula
- C10H11BrO2
- Formula Weight
- 243.1
- MOL File
- 2178-24-7.mol
Ethyl 2-(2-bromophenyl)acetate Property
- Melting point:
- 35-38℃
- Boiling point:
- 114 °C(Press: 4 Torr)
- Density
- 1.389±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to off-white <35°C Solid,>36°C Liquid
Safety
- RIDADR
- UN3261
- HazardClass
- 8
- PackingGroup
- II
- HS Code
- 2915390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- E937095
- Product name
- Ethyl2-(2-Bromophenyl)acetate
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- J95443
- Product name
- Ethyl(2-bromophenyl)acetate
- Packaging
- 1g
- Price
- $20
- Updated
- 2021/12/16
- Product number
- 7415AD
- Product name
- Ethyl(2-bromophenyl)acetate
- Packaging
- 1g
- Price
- $27
- Updated
- 2021/12/16
- Product number
- 066805
- Product name
- Ethyl(2-bromophenyl)acetate
- Purity
- 97%
- Packaging
- 5g
- Price
- $30
- Updated
- 2021/12/16
- Product number
- 083329
- Product name
- Ethyl (2-bromophenyl)acetate
- Purity
- 97%
- Packaging
- 1g
- Price
- $194
- Updated
- 2021/12/16
Ethyl 2-(2-bromophenyl)acetate Chemical Properties,Usage,Production
Uses
ETHYL 2-(2-BROMOPHENYL)ACETATE is a useful research chemical.
Synthesis
64-17-5
18698-97-0
2178-24-7
GENERAL METHOD: 3 g (13.8 mmol) of o-bromophenylacetic acid was dissolved in 10 mL of ethanol and the solution was cooled to 0°C. The solution was then cooled to 0°C and the solution was then dried. Under stirring, 1.6 mL (22 mmol) of thionyl chloride was slowly added dropwise. After the dropwise addition was completed, the reaction mixture was gradually heated to 50 °C and kept at this temperature for the reaction overnight. Upon completion of the reaction, the mixture was cooled to room temperature and the solvent was subsequently evaporated under reduced pressure. The residue was mixed with ethyl acetate and filtered through a 6 g column of basic alumina. Finally, the filtrate was evaporated under reduced pressure to give 3.5 g (89% yield) of ethyl (2-bromophenyl) acetate (1d).
References
[1] European Journal of Inorganic Chemistry, 2015, vol. 2015, # 10, p. 1752 - 1758
[2] Patent: WO2009/121919, 2009, A1. Location in patent: Page/Page column 163
[3] Synthesis (Germany), 2015, vol. 47, # 13, p. 1913 - 1921
[4] Organic Letters, 2005, vol. 7, # 22, p. 4963 - 4966
[5] Patent: WO2004/63150, 2004, A2. Location in patent: Page 28
Ethyl 2-(2-bromophenyl)acetate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethyl 2-(2-bromophenyl)acetate manufacturers
- Product
- Ethyl 2-(2-bromophenyl)acetate 2178-24-7
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27