N-Methyl-(5-bromopyrid-3-yl)methylamine

Product Name: N-Methyl-(5-bromopyrid-3-yl)methylamine
CAS No.: 73335-64-5
Chemical Name: N-Methyl-(5-bromopyrid-3-yl)methylamine
Synonyms: 1-(5-Bromopyridin-3-yl);5-bromo-N-methyl-3-Pyridinemethan amine;3-Bromo-5-[(methylamino)methyl]pyridine;N-Methyl-(5-bromopyrid-3-yl)methylamine;3-Pyridinemethanamine, 5-bromo-N-methyl-;(5-Bromopyridin-3-yl)-N-methylmethylamine;3-Bromo-5-[(methylamino)methyl]pyridine95%;1-(5-bromo-3-pyridinyl)-N-methylmethanamine;1-(5-broMopyridin-2-yl)-N-MethylMethanaMine;1-(5-bromopyridin-3-yl)-N-methylmethanamine
CBNumber: CB6854168
Molecular Formula: C7H9BrN2
Formula Weight: 201.06
MOL File: 73335-64-5.mol

More

Less

N-Methyl-(5-bromopyrid-3-yl)methylamine Property

Boiling point:: 125 °C
storage temp.: Keep in dark place,Inert atmosphere,Room temperature

More

Less

Safety

Hazard Codes: C
Hazard Note: Corrosive
HS Code: 2933599590

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: B704028
Product name: 1-(5-Bromopyridin-3-yl)-N-methylmethanamine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-9-09
Product name: 3-Bromo-5-[(methylamino)methyl]pyridine
Purity: 95%
Packaging: 250mg
Price: $168
Updated: 2021/12/16

Matrix Scientific

Product number: 075846
Product name: 1-(5-Bromopyridin-3-yl)-N-methylmethanamine
Purity: 95+%
Packaging: 500mg
Price: $240
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-9-09
Product name: 3-Bromo-5-[(methylamino)methyl]pyridine
Purity: 95%
Packaging: 1g
Price: $400
Updated: 2021/12/16

Matrix Scientific

Product number: 075846
Product name: 1-(5-Bromopyridin-3-yl)-N-methylmethanamine
Purity: 95+%
Packaging: 1g
Price: $416
Updated: 2021/12/16

More

Less

N-Methyl-(5-bromopyrid-3-yl)methylamine Chemical Properties,Usage,Production

Synthesis

113118-81-3

593-51-1

73335-64-5

GENERAL STEPS: 1.8 g (27 mmol) of methylamine hydrochloride and 0.4 g (6 mmol) of sodium cyanoborohydride were added sequentially to a 20 mL methanol solution containing 1 g (5.4 mmol) of 5-bromopyridine-3-carbaldehyde. The reaction mixture was stirred at room temperature for 48 hours. After completion of the reaction, the precipitate was removed by filtration and the filtrate was concentrated to dryness under reduced pressure. The residue was dissolved in dichloromethane and washed with deionized water. After separating the organic phase, the organic phase was washed with dilute aqueous hydrochloric acid. The acid-washed aqueous phase was adjusted to pH 9 with aqueous sodium hydroxide and subsequently extracted with dichloromethane. The organic phases were combined, dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with dichloromethane/methanol (9.5:0.5, v/v) as eluent. 0.5 g (50% yield) of N-methyl-(5-bromopyridin-3-yl)methylamine was finally obtained.

References

[1] Patent: WO2004/113331, 2004, A1. Location in patent: Page 44-45

N-Methyl-(5-bromopyrid-3-yl)methylamine Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

N-Methyl-(5-bromopyrid-3-yl)methylamine Suppliers

Belgium 1 CHINA 29 India 1 United Kingdom 1 United States 5 Global 37

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Tetranov Biopharm

Tel: 13526569071
Email: sales@leadmedpharm.com
Country: China
ProdList: 7892
Advantage: 64

Thermo Fisher Scientific

Tel: 800-810-5118
Fax: +86-10-84193589
Email: cnchemical@thermofisher.com
Country: China
ProdList: 17770
Advantage: 75

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

9ding chemical ( Shanghai) Limited

Tel: 4009209199
Fax: 86-021-52271987
Email: sales@9dingchem.com
Country: China
ProdList: 22514
Advantage: 55

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Shanghai Hong-chuang Pharma Tech Co., Ltd.

Tel: 18151128828
Fax: -
Email: hc-sales@foxmail.com
Country: China
ProdList: 2647
Advantage: 55

Tianjin Anhao Biological Technology Co., Ltd.

Tel
Email: sales@ahpharmatech.com
Country: China
ProdList: 5734
Advantage: 55

Shanghai Boyners Pharm-Tech Co., Ltd.

Tel: 13817873692
Fax: 021-31329586
Email: mkt@boynerspharm.com
Country: China
ProdList: 1707
Advantage: 55

Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd

Tel: 18210788515
Fax: 18210788515
Email: zhuzixin999@163.c0m
Country: China
ProdList: 2998
Advantage: 55

73335-64-5, N-Methyl-(5-bromopyrid-3-yl)methylamineRelated Search:

5-BROMO-N-TERT-BUTYLNICOTINAMIDE (5-BROMOPYRIDIN-3-YL)-MORPHOLIN-4-YL-METHANONE 5-BROMO-N,N-DIMETHYL-3-PYRIDINECARBOXAMIDE 5-BROMO-N,N-DIETHYL-3-PYRIDINECARBOXAMIDE 1-(5-BROMO-PYRIDINE-3-CARBONYL)-PYRROLIDINE-2-CARBOXYLIC ACID 5-BROMO-3-(PIPERIDIN-1-YLCARBONYL)PYRIDINE TCV 309 N-Benzyl-5-bromo-nicotinamide 5-Bromo-N-methyl-nicotinamide 5-bromo-N-(2-bromo-4-methylphenyl)pyridine-3-carboxamide AURORA 22740 4-[(5-bromopyridin-3-yl)formamido]butanoic acid AURORA 1932 AURORA 22741 AURORA 22743 5-bromo-N-(4-bromophenyl)pyridine-3-carboxamide AURORA 10464 AURORA 22739

N-Methyl-(5-bromopyrid-3-yl)methylamine

3-Bromo-5-[(methylamino)methyl]pyridine

3-Bromo-5-[(methylamino)methyl]pyridine 95%

1-(5-bromopyridin-3-yl)-N-methylmethanamine

1-(5-broMopyridin-2-yl)-N-MethylMethanaMine

5-bromo-N-methyl-3-Pyridinemethan amine

3-Bromo-5-[(methylamino)methyl]pyridine95%

1-(5-Bromopyridin-3-yl)

(5-Bromopyridin-3-yl)-N-methylmethylamine

1-(5-bromo-3-pyridinyl)-N-methylmethanamine

3-Pyridinemethanamine, 5-bromo-N-methyl-

73335-64-5