ChemicalBook > CAS DataBase List > 3-bromo-5-methylaniline
3-bromo-5-methylaniline
- Product Name
- 3-bromo-5-methylaniline
- CAS No.
- 74586-53-1
- Chemical Name
- 3-bromo-5-methylaniline
- Synonyms
- 3-AMino-5-broMotoluene;3-bromo-5-methylaniline;3-Bromo-5-methylbenzenamine;3-Bromo-5-methylaniline,98%;BenzenaMine,3-broMo-5-Methyl-;3-Amino-5-bromotoluene, 5-Bromo-m-toluidine
- CBNumber
- CB6908751
- Molecular Formula
- C7H8BrN
- Formula Weight
- 186.05
- MOL File
- 74586-53-1.mol
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3-bromo-5-methylaniline Property
- Melting point:
- 37 °C
- Boiling point:
- 150-151 °C(Press: 15 Torr)
- Density
- 1.498±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Powder
- pka
- 3.65±0.10(Predicted)
- color
- Brown
- Water Solubility
- Slightly soluble in water.
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Safety
- HazardClass
- 6.1
- HS Code
- 2921430090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
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N-Bromosuccinimide Price
TCI Chemical
- Product number
- B6015
- Product name
- 3-Bromo-5-methylaniline
- Packaging
- 5G
- Price
- $157
- Updated
- 2025/07/31
TCI Chemical
- Product number
- B6015
- Product name
- 3-Bromo-5-methylaniline
- Packaging
- 25G
- Price
- $626
- Updated
- 2025/07/31
TRC
- Product number
- B814220
- Product name
- 3-Bromo-5-methylaniline
- Packaging
- 10g
- Price
- $200
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 3730-9-Y1
- Product name
- 3-Bromo-5-methylaniline
- Packaging
- 2g
- Price
- $15
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 3730-9-Y1
- Product name
- 3-Bromo-5-methylaniline
- Packaging
- 5G
- Price
- $30
- Updated
- 2021/12/16
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3-bromo-5-methylaniline Chemical Properties,Usage,Production
Uses
3-Bromo-5-methylaniline is used as pharmaceutical intermediates and chemical intermediate.
Synthesis
52488-28-5
74586-53-1
General procedure for the synthesis of 3-bromo-5-methylaniline from 3-bromo-5-nitrotoluene: 1-bromo-3-methyl-5-nitrobenzene (5 g, 23.1 mmol) was dissolved in a mixed solvent of dioxane/water (3:1, 40 mL), and zinc powder (15 g, 231 mmol) and ammonium chloride (12.3 g, 231 mmol) were added sequentially. The reaction mixture was stirred at room temperature for 4 hours. After completion of the reaction, the reaction mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 3-bromo-5-methylaniline (4.0 g, 93% yield) as a brown solid. Mass spectrometry analysis showed m/z (M+H) of 186.2.
References
[1] Patent: WO2014/149164, 2014, A1. Location in patent: Paragraph 001105
[2] Chemische Berichte, 1880, vol. 13, p. 963
[3] Chemische Berichte, 1881, vol. 14, p. 417
[4] Justus Liebigs Annalen der Chemie, 1878, vol. 192, p. 203
[5] Journal of the Chemical Society, 1929, p. 1255
3-bromo-5-methylaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-bromo-5-methylaniline manufacturers
Career Henan Chemical Co
- Product
- 3-bromo-5-methylaniline 74586-53-1
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- JD724
- Release date
- 2019-09-02