ChemicalBook > CAS DataBase List > Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)

Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)

Product Name
Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
CAS No.
30152-05-7
Chemical Name
Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
Synonyms
1-(3-Hydroxypyridin-4-yl);4-ACETYL-3-HYDROXYPYRIDINE;1-(3-hydroxy-4-pyridyl)ethanone;3-hydroxy-4-pyridylmethyl ketone;1-(3-Hydroxypyridin-4-yl)ethanone;1-(3-Hydroxy-4-pyridinyl)ethanone;1-(3-hydroxypyridin-4-yl)ethan-1-one;Ethanone, 1-(3-hydroxy-4-pyridinyl)-;Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
CBNumber
CB71066064
Molecular Formula
C7H7NO2
Formula Weight
137.14
MOL File
30152-05-7.mol
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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Property

Melting point:
52-54℃
Boiling point:
336.5±22.0 °C(Predicted)
Density 
1.217±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
6.90±0.10(Predicted)
Appearance
Yellow to brown Solid
InChI
InChI=1S/C7H7NO2/c1-5(9)6-2-3-8-4-7(6)10/h2-4,10H,1H3
InChIKey
REYSBWKWFPSDDR-UHFFFAOYSA-N
SMILES
C(=O)(C1C=CN=CC=1O)C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
A416805
Product name
1-(3-Hydroxypyridin-4-yl)ethanone
Packaging
50mg
Price
$90
Updated
2021/12/16
TRC
Product number
A416805
Product name
1-(3-Hydroxypyridin-4-yl)ethanone
Packaging
100mg
Price
$130
Updated
2021/12/16
ChemScene
Product number
CS-B0938
Product name
Ethanone,1-(3-hydroxy-4-pyridinyl)-
Purity
99.96%
Packaging
250mg
Price
$136
Updated
2021/12/16
AK Scientific
Product number
Z4577
Product name
1-(3-Hydroxypyridin-4-yl)ethanone
Packaging
100mg
Price
$171
Updated
2021/12/16
ChemScene
Product number
CS-B0938
Product name
Ethanone,1-(3-hydroxy-4-pyridinyl)-
Purity
99.96%
Packaging
1g
Price
$300
Updated
2021/12/16
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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Chemical Properties,Usage,Production

Synthesis

1089689-12-2

30152-05-7

Synthesis of Intermediate IV: Intermediate III (6 g, 33.114 mmol, 1 eq.) was dissolved in EtOH (96 mL), followed by addition of 5 M hydrochloric acid (53 mL). The reaction mixture was stirred at room temperature for 16 hours. Upon completion of the reaction, the solvent was removed by evaporation and the residue was dissolved in MeOH, added to silica gel and evaporated again. Purification by fast chromatography (Biotage, eluent 0% to 20% MeOH in DCM solution) gave Intermediate IV (4.5 g, 99% yield) in orange solid form. The product was analyzed by HPLC-MS (Method 4): retention time Rt = 0.7, [M + H]+ 138.1.1. 1H NMR (300 MHz, DMSO) δ 8.58 (s, 1H), 8.33 (d, J = 4.9 Hz, 1H), 7.80 (d, J = 5.3 Hz, 1H), 2.64 (s, 3H).

References

[1] Patent: WO2017/33019, 2017, A1. Location in patent: Page/Page column 69; 70
[2] Patent: WO2014/141110, 2014, A2. Location in patent: Page/Page column 97

Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) Suppliers

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View Lastest Price from Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) 30152-05-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-07-18
Career Henan Chemical Co
Product
Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI) 30152-05-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-02

30152-05-7, Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)Related Search:


  • Ethanone, 1-(3-hydroxy-4-pyridinyl)- (9CI)
  • 4-ACETYL-3-HYDROXYPYRIDINE
  • 1-(3-Hydroxypyridin-4-yl)ethanone
  • Ethanone, 1-(3-hydroxy-4-pyridinyl)-
  • 1-(3-Hydroxy-4-pyridinyl)ethanone
  • 3-hydroxy-4-pyridylmethyl ketone
  • 1-(3-Hydroxypyridin-4-yl)
  • 1-(3-hydroxy-4-pyridyl)ethanone
  • 1-(3-hydroxypyridin-4-yl)ethan-1-one
  • 30152-05-7
  • ACETYLGROUP