ChemicalBook > CAS DataBase List > Benzonitrile, 5-amino-2-methoxy- (9CI)

Benzonitrile, 5-amino-2-methoxy- (9CI)

Product Name: Benzonitrile, 5-amino-2-methoxy- (9CI)
CAS No.: 214623-57-1
Chemical Name: Benzonitrile, 5-amino-2-methoxy- (9CI)
Synonyms: Albb-004948;3-Cyano-4-methoxyaniline;2-Methoxy-5-amnobenzonitrile;2-Methoxy-5-aMinobenzonitrile;5-amino-2-methoxybenzonitrile;Benzonitrile, 5-amino-2-methoxy-;5-Amino-2-methoxybenzonitrile 98%;Benzonitrile, 5-amino-2-methoxy- (9CI);5-amino-2-methoxybenzonitrile(SALTDATA: FREE)
CBNumber: CB71071406
Molecular Formula: C8H8N2O
Formula Weight: 148.16
MOL File: 214623-57-1.mol

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Benzonitrile, 5-amino-2-methoxy- (9CI) Property

Melting point:: 100 °C
Boiling point:: 347.5±22.0 °C(Predicted)
Density: 1.17±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: Solid
pka: 3.39±0.10(Predicted)
Appearance: Brown to gray Solid
InChI: InChI=1S/C8H8N2O/c1-11-8-3-2-7(10)4-6(8)5-9/h2-4H,10H2,1H3
InChIKey: BZNMIDYUSWEPOM-UHFFFAOYSA-N
SMILES: C(#N)C1=CC(N)=CC=C1OC

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Safety

HazardClass: IRRITANT
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A612473
Product name: 5-amino-2-methoxybenzonitrile
Packaging: 500mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: 0917AB
Product name: 2-Methoxy-5-aminobenzonitrile
Packaging: 1g
Price: $181
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4637-1-17
Product name: 5-Amino-2-methoxybenzonitrile
Packaging: 1g
Price: $184
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA116318
Product name: 5-Amino-2-methoxybenzonitrile
Packaging: 500mg
Price: $200
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA116318
Product name: 5-Amino-2-methoxybenzonitrile
Packaging: 100mg
Price: $58
Updated: 2021/12/16

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Benzonitrile, 5-amino-2-methoxy- (9CI) Chemical Properties,Usage,Production

Synthesis

10496-75-0

214623-57-1

General procedure for the synthesis of 5-amino-2-methoxybenzonitrile from 2-methoxy-5-nitrobenzonitrile: 2-methoxy-5-nitrobenzonitrile (1 equiv., 220 mg, 1.23 mmol), methanol (20 mL), and carbon-carrying palladium (10% mass, 10 mg) were added sequentially to a 100 mL round-bottom flask. The flask was connected to a three-way system and the reaction was stirred at room temperature. Evacuation was carried out and then filled with nitrogen, and this cycle was repeated three times, each time the nitrogen was filled for not less than 5 minutes. The reaction was allowed to proceed at room temperature for 30 minutes under hydrogen protection. Upon completion of the reaction, the palladium-carbon catalyst was removed by filtration, the filtrate was concentrated and purified by column chromatography (petroleum ether:ethyl acetate = 5:1) to afford 150 mg of the target product 5-amino-2-methoxybenzonitrile (Compound 7) as a white crystalline solid in 82% yield.

References

[1] Patent: CN106892871, 2017, A. Location in patent: Paragraph 0109; 0112; 0113
[2] Patent: CN105294584, 2016, A. Location in patent: Paragraph 0018; 0019
[3] Journal of the Chemical Society, 1945, p. 861,864
[4] Chemical Biology and Drug Design, 2018, vol. 91, # 2, p. 526 - 533

Benzonitrile, 5-amino-2-methoxy- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Benzonitrile, 5-amino-2-methoxy- (9CI) manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: Benzonitrile, 5-amino-2-methoxy- (9CI) 214623-57-1
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-06

Henan Bao Enluo International TradeCo.，LTD

Product: Benzonitrile, 5-amino-2-methoxy- (9CI) 214623-57-1
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 10000MT
Release date: 2023-08-08

Career Henan Chemical Co

Product: Benzonitrile, 5-amino-2-methoxy- (9CI) 214623-57-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-12-20

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Benzonitrile, 5-amino-2-methoxy- (9CI)

Albb-004948

5-amino-2-methoxybenzonitrile(SALTDATA: FREE)

5-amino-2-methoxybenzonitrile

2-Methoxy-5-aMinobenzonitrile

3-Cyano-4-methoxyaniline

5-Amino-2-methoxybenzonitrile 98%

Benzonitrile, 5-amino-2-methoxy-

2-Methoxy-5-amnobenzonitrile

214623-57-1

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