3,4-PYRIDINEDICARBOXIMIDE

Product Name: 3,4-PYRIDINEDICARBOXIMIDE
CAS No.: 4664-01-1
Chemical Name: 3,4-PYRIDINEDICARBOXIMIDE
Synonyms: 1H-PYRROLO[3,4-C]PYRIDINE-1,3(2H)-DIONE;CINCHOMERONIMIDE;4-azaphthalimid;BUTTPARK 48\06-51;TIMTEC-BB SBB004086;cinchomeronicacidimide;3,4-Pyridinedicarbimide;Pyridine-3,4-dicarbimide;3,4-PYRIDINEDICARBOXIMIDE;Pyridine-3,4-dicarboxiMide
CBNumber: CB7123621
Molecular Formula: C7H4N2O2
Formula Weight: 148.12
MOL File: 4664-01-1.mol

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3,4-PYRIDINEDICARBOXIMIDE Property

Melting point:: 232-235 °C(lit.)
Boiling point:: 268.69°C (rough estimate)
Density: 1.4015 (rough estimate)
refractive index: 1.5300 (estimate)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 7.80±0.20(Predicted)
form: Crystalline Powder
color: White to tan
InChI: InChI=1S/C7H4N2O2/c10-6-4-1-2-8-3-5(4)7(11)9-6/h1-3H,(H,9,10,11)
InChIKey: SJSABZBUTDSWMJ-UHFFFAOYSA-N
SMILES: C1=NC=CC2C(=O)NC(=O)C1=2

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
WGK Germany: 3
RTECS: US7966000
HazardClass: IRRITANT
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: P992203
Product name: Pyridine-3,4-dicarboximide
Packaging: 500mg
Price: $60
Updated: 2021/12/16

TRC

Product number: P992203
Product name: Pyridine-3,4-dicarboximide
Packaging: 2.5g
Price: $75
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK226074
Product name: 3,4-Pyridinedicarboximide
Purity: 97%
Packaging: 5g
Price: $64
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK226074
Product name: 3,4-Pyridinedicarboximide
Purity: 97%
Packaging: 1g
Price: $16
Updated: 2021/12/16

Matrix Scientific

Product number: 059237
Product name: 3,4-Pyridinedicarboximide
Purity: 95+%
Packaging: 1g
Price: $32
Updated: 2021/12/16

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3,4-PYRIDINEDICARBOXIMIDE Chemical Properties,Usage,Production

Chemical Properties

White to light brown powder

Synthesis

490-11-9

4664-01-1

The general procedure for the synthesis of 3,4-pyridinedicarboxylic acid as a raw material for the synthesis of 3,4-pyridinedicarboximides was as follows: firstly, sublimated 3,4-pyridinedicarboxylic acid (50 g, 300 mmol) was suspended in acetic anhydride (123.5 g, 1,200 mmol), and heated to reflux (140-150 °C) until the solid was completely dissolved and the mixture presented homogeneous state. Subsequently, the reaction mixture was cooled and concentrated under vacuum. Next, acetamide (50 g, 846 mmol) was added to the concentrate and the mixture was heated and reacted at 140 °C for 3 hours. After completion of the reaction, the mixture was cooled to room temperature. The solid residue formed during cooling was pulverized, ground with 100 ml of water, filtered and washed with additional water. Finally, the resulting solid was dried in a desiccator to afford 3,4-pyridinedicarboximide (42.26 g, 95.1% yield), which met the purity requirements for use without further purification. The product was analyzed by LC-MS showing a m/z (ESP) of 149 [M + H]+ and a retention time (R/T) of 0.44 min.

References

[1] Patent: US2006/199804, 2006, A1. Location in patent: Page/Page column 29
[2] Acta Chimica Hungarica, 1983, vol. 112, # 4, p. 487 - 500

3,4-PYRIDINEDICARBOXIMIDE Preparation Products And Raw materials

Raw materials

Acetic anhydride Acetamide 3,4-Pyridinedicarboxylic acid

Preparation Products

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3,4-PYRIDINEDICARBOXIMIDE Suppliers

Canada 1 China 71 Germany 2 India 2 Switzerland 1 The Netherlands 1 United Kingdom 4 United States 21 Global 103

Suzhou Nuoouman Biological Technology Co., Ltd.

Tel: 15026866316
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J & K SCIENTIFIC LTD.

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Meryer (Shanghai) Chemical Technology Co., Ltd.

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Fax: 86-21-61259102
Email: market03@meryer.com
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Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
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Energy Chemical

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Pure Chemistry Scientific Inc.

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Shandong Xiya Chemical Co., Ltd

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Hangzhou Yuhao Chemical Technology Co., Ltd

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Thermo Fisher Scientific

Tel: 800-810-5118
Fax: +86-10-84193589
Email: cnchemical@thermofisher.com
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View Lastest Price from 3,4-PYRIDINEDICARBOXIMIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3,4-Pyridinedicarboximide 4664-01-1
Price: US $1.00-22.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100000KG
Release date: 2024-07-31

4664-01-1, 3,4-PYRIDINEDICARBOXIMIDERelated Search:

3,4-PYRIDINEDICARBOXIMIDE 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione N-Benzyl- 2,3-pyridinedicarboximide 2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE 4-CHLORO-6-METHYL-2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-1,3-DIONE 4-Chloro-6-methyl-2-(4-methylbenzyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione 4-chloro-2-(2-chloro-6-fluoroBenzyl)-6-methyl-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione 4-METHYL-2,3-DIHYDRO-1H-PYRROLO[3,4-C]QUINOLINE-1,3-DIONE 4-Chloro-6-methyl-2-[3-(trifluoromethyl)Benzyl]-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide N-(2,6-dimethylphenyl)-3,4-pyridinedicarboximide 2,3-Pyridinedicarboximide, N-(5,5-dimethyl-2-oxotetrahydro-3-furyl)- 6-(TERT-BUTYL)-4-CHLORO-2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-1,3-DIONE 4-chloro-2-(2,4-dichlorobenzyl)-6-methyl-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione 2-benzyl-4-chloro-6-methyl-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione 2-[[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL](METHYL)AMINO]-1H-PYRROLO[3,4-C]PYRIDINE-1,3(2H)-DIONE 4-[(CHLOROMETHYL)THIO]-6-METHYL-2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-1,3-DIONE METHYL 2-BENZYL-7-HYDROXY-1,3-DIOXO-2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-4-CARBOXYLATE

3,4-PYRIDINEDICARBOXIMIDE

1H-PYRROLO[3,4-C]PYRIDINE-1,3(2H)-DIONE

2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-1,3-DIONE

CINCHOMERONIMIDE

BUTTPARK 48\06-51

3,4-Pyridinedicarboximide ,97%

2H-Pyrrolo[3,4-c]pyridine-1,3-dione

3,4-Pyridinedicarbimide

Pyridine-3,4-dicarbimide

pyrrolo[3,4-c]pyridine-1,3-quinone

1H-Pyrrolo[3,4-c]pyridine-1,3(2H)-dione 99%

Pyridine-3,4-dicarboxiMide

Pyridine-3,4-dicarboximide, Cinchomeronimide, 2,3-Dihydro-1H-pyrrolo[3,4-c]pyridine-1,3-dione

1H,2H,3H-pyrrolo[3,4-c]pyridine-1,3-dione

1H-pyrrolo[3,4-c]pyridine-1,3(2H)-dione/3,4-pyridinedicarboxiMide

1H-Pyrrolo[3,4-c]pyridine-1,3(2H)-dione, Cinchomeronimide, 2,3-Dihydro-1,3-dioxo-1H-pyrrolo[3,4-c]pyridine

Pyridine-3,4-dicarboximide 99%

4-azaphthalimid

cinchomeronicacidimide

TIMTEC-BB SBB004086

PYRROLO[3,4-C]PYRIDINE-1,3-DIONE

3,4 3,4-Pyridinedicarboximide-Pyridinedicarboximide

4664-01-1

AMINE