METHANOL-D3

Product Name: METHANOL-D3
CAS No.: 1849-29-2
Chemical Name: METHANOL-D3
Synonyms: CD3OH;METHANOL-D3;METHAN-D3-OL;METHANOL-D3OH;(2H3)methanol;MethanolD3>99.8%;METHYL-D3 ALCOHOL;(1,1,1-2H3)Methanol;Hydroxy(2H3)methane;TETRADEUTEROMETHANOL
CBNumber: CB7126273
Molecular Formula: CHD3O
Formula Weight: 35.06
MOL File: 1849-29-2.mol

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METHANOL-D3 Property

Melting point:: 174-177 °C
Melting point:: -97,8°C
Boiling point:: 64,7°C
Boiling point:: 65 °C (lit.)
Density: 0.867 g/mL at 25 °C (lit.)
Density: d = 0,86
vapor pressure: 129 hPa ( 20 °C)
refractive index: n20/D 1.327(lit.)
Flash point:: 52 °F
storage temp.: Flammables area
solubility: soluble in Chloroform
form: Liquid
color: Colorless
explosive limit: 5.5-36.5%(V)
BRN: 1732010
InChI: 1S/CH4O/c1-2/h2H,1H3/i1D3
InChIKey: OKKJLVBELUTLKV-FIBGUPNXSA-N
CAS Number Unlabeled: 67-56-1

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Safety

Hazard Codes: F,T
Risk Statements: 11-23/25-39/23/24/25-23/24/25
Safety Statements: 7-16-24-45-36/37
RIDADR: UN 1230 3/PG 2
WGK Germany: 3
F: 10
Autoignition Temperature: 440°C
HS Code: 28459000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H225Highly Flammable liquid and vapour

H370Causes damage to organs

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 343854
Product name: Methanol-d3
Purity: 99.8 atom % D
Packaging: 1g
Price: $71.4
Updated: 2025/07/31

Sigma-Aldrich

Product number: 343854
Product name: Methanol-d3
Purity: 99.8 atom % D
Packaging: 5g
Price: $260
Updated: 2025/07/31

Sigma-Aldrich

Product number: 343854
Product name: Methanol-d3
Purity: 99.8 atom % D
Packaging: 10g
Price: $451
Updated: 2025/07/31

TRC

Product number: M276588
Product name: Methanol-d3
Packaging: 1g
Price: $65
Updated: 2021/12/16

Usbiological

Product number: 454473
Product name: Methanol-d3
Packaging: 1g
Price: $340
Updated: 2021/12/16

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METHANOL-D3 Chemical Properties,Usage,Production

Chemical Properties

clear colorless liquid

Uses

Methanol-d₃ may be used in the preparation of [Al(CH₃)2OCD₃]₃ by reacting with trimethylaluminum for use in spectroscopic analysis of dialkylaluminum alkoxides and the trialkylaluminum-ether complex.

General Description

Methanol-d₃ is a deuterated NMR solvent that is useful in NMR-based research and analyses.

Synthesis

The method of preparing fully deuterated methanol (methanol-D3) is as follows: opening the valves of deuterium gas and carbon monoxide, controlling the volume ratio of 1:1 to pre-mix first (deuterium gas and carbon monoxide are 2kg and 14kg respectively, totaling 16kg). Under the pressure of 5.5MPa, the catalyst bed of gold oxide: platinum oxide: rhodium oxide = 1:3:2 (mass ratio) was passed through 210~380??C at the speed of 2L/sec. After 24 hours of continuous cyclic reaction, the fully deuterated methanol (methanol-D3) reaction solution was obtained in the separation kettle, and the obtained reaction solution, after distillation, was prepared as fully deuterated methanol (methanol-D3): 3.2kg, with the yield of 35.5%, GC purity 99.8%. Theoretical value of elemental analysis: C33.30%, D22.34%, O44.36%; measured value: C33.32%, D22.33%, O44.35%.

METHANOL-D3 Preparation Products And Raw materials

Raw materials

Preparation Products

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METHANOL-D3 Suppliers

Belgium 1 Canada 1 China 36 France 1 Germany 2 India 2 Japan 2 Switzerland 1 United Kingdom 3 United States 9 Global 58

J & K SCIENTIFIC LTD.

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Thermo Fisher Scientific

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Sigma-Aldrich

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Shanghai Qiao Chemical Science Co., Ltd

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Shandong Xiya Chemical Co., Ltd.

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1849-29-2, METHANOL-D3Related Search:

METHYL-D3 P-TOLUENESULFONATE DIMETHYL-D6 SULFATE BIS(2-METHOXYETHYL) ETHER-D14 (1,4-DIMETHYL-2-PIPERAZINYL)METHANOL,(1,4-DIMETHYLPIPERAZIN-2-YL)METHANOL Bromoacetaldehyde dimethyl acetal 3-Ethyl-3-pentanol Tulobuterol hydrochloride Acetoin Pyridine 2-METHYL-2-HEPTANOL METARAMINOL (1,5-DIMETHYL-1H-PYRAZOL-3-YL)METHANOL GUAI-1(5)-EN-11-OL:ACETATE 4-Methylbenzhydrol 18-CROWN-6-METHANOL 3-METHYL-2-BUTANOL Dimethoxymethane Methanol-d4

TETRADEUTEROMETHANOL

METHYL-D3 ALCOHOL

METHAN-D3-OL

METHANOL-D3

METHANOL-D3OH

MethanolD3>99.8%10X0.75ml

MethanolD3>99.8%

1,1,1-trideuteromethanol

C,C,C-trideuterio-methanol

Methanol-D3 >99.5 Atom % D

1,1,1-Trideuteromethanol, Methyl-d3 alcohol

(1,1,1-2H3)Methanol

Hydroxy(2H3)methane

Methanol-d3,for NMR,99.5 atom % D

Methanol-d3Methyl-d3 alcohol1,1,1-Trideuteromethanol

METHANOL-D3 DEUTERATION MAGNISOLV(TM)

(2H3)methanol

METHANOL-D3, 99.8 ATOM % D

METHANOL-D3 DEUTERATION DEGREE MIN. 99 A TOM % D

Methanol-d3, 99.5 atom % D, for NMR

CD3OH

Methanol-d<sub>3</sub>

Methanol-D3 >99.5 Atom % D 1ml ampoule

Methanol-D3 >99.5 Atom % D 5ml Bottle

Methanol (D?, 99.5%)

1849-29-2

CHD3O

BioChemical

Alphabetical Listings

Stable Isotopes