ChemicalBook > CAS DataBase List > 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1

3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1

Product Name: 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1
CAS No.: 1668-53-7
Chemical Name: 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1
Synonyms: DBDT;UV-107;UV-1168;Doxepin for system suitability CRS;3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-...;4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-3-benzenediol;3-benzenediol,4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl];4-[4,6-Bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1,3-Benzenediol;2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine;4-(4,6-Bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol
CBNumber: CB71453884
Molecular Formula: C25H23N3O2
Formula Weight: 397.47
MOL File: 1668-53-7.mol

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3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Property

Melting point:: 203.0 to 207.0 °C
Boiling point:: 659.1±65.0 °C(Predicted)
Density: 1?+-.0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: soluble in Dimethylformamide
form: powder to crystal
pka: 8.58±0.40(Predicted)
color: White to Light yellow to Light orange
InChI: InChI=1S/C25H23N3O2/c1-14-5-8-19(16(3)11-14)23-26-24(20-9-6-15(2)12-17(20)4)28-25(27-23)21-10-7-18(29)13-22(21)30/h5-13,29-30H,1-4H3
InChIKey: FROCQMFXPIROOK-UHFFFAOYSA-N
SMILES: C1(O)=CC=C(C2=NC(C3=CC=C(C)C=C3C)=NC(C3=CC=C(C)C=C3C)=N2)C(O)=C1
EPA Substance Registry System: 1,3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]- (1668-53-7)

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Safety

HS Code: 2933.69.6050

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4527
Product name: 2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Purity: >98.0%(HPLC)(N)
Packaging: 5g
Price: $103
Updated: 2025/07/31

TCI Chemical

Product number: D4527
Product name: 2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Purity: >98.0%(HPLC)(N)
Packaging: 25g
Price: $344
Updated: 2025/07/31

TRC

Product number: D458318
Product name: 2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: D458318
Product name: 2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD159256
Product name: 2-(2,4-Dihydroxyphenyl)-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazine
Packaging: 2g
Price: $60
Updated: 2021/12/16

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3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Chemical Properties,Usage,Production

Synthesis

1237-53-2

108-46-3

1668-53-7

The general procedure for the synthesis of 4-(4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol from 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol using 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl and resorcinol was carried out as follows: in a 50 mL three-necked flask protected by a dry nitrogen gas, 2-chloro-4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-1,3,5-triazin-2-yl (1.6 mmol) and 2-chloro-4,6 -bis(2,4-dimethylphenyl)-1,3,5-triazine (1.6 mmol) and anhydrous aluminum trichloride (0.32 g, 2.4 mmol) to anhydrous chlorobenzene (15 mL), and the reaction mixture was stirred for 0.5 hours at 25 °C. Subsequently, resorcinol (0.24 g, 2.2 mmol) was added and the reaction mixture was warmed up to 85 °C for continued stirring for 5 hours. Upon completion of the reaction, it was cooled to room temperature and the reaction was quenched by the slow addition of ice water (10 mL), followed by evaporation under reduced pressure to remove the chlorobenzene. The mixture was filtered and the resulting solid was washed with water (3 x 10 mL) and finally recrystallized from ethyl acetate to afford the target product 4-(4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl)benzene-1,3-diol and its derivatives.

References

[1] Journal of Fluorescence, 2018, vol. 28, # 2, p. 707 - 723
[2] Patent: US6242598, 2001, B1

3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 manufacturers

Career Henan Chemical Co

Product: 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1 1668-53-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2018-08-09

1668-53-7, 3-Benzenediol, 4-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-1Related Search:

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1668-53-7