N,N-dimethyl-1-(4-nitrophenyl)methanamine
- Product Name
- N,N-dimethyl-1-(4-nitrophenyl)methanamine
- CAS No.
- 15184-96-0
- Chemical Name
- N,N-dimethyl-1-(4-nitrophenyl)methanamine
- Synonyms
- N,N-Dimethyl-1-(4-nitrophenyl);N,N-DiMethyl-4-nitrobenzylaMine;Benzenemethanamine, N,N-dimethyl-4-nitro-;N,N-dimethyl-1-(4-nitrophenyl)methanamine
- CBNumber
- CB71457024
- Molecular Formula
- C9H12N2O2
- Formula Weight
- 180.2
- MOL File
- 15184-96-0.mol
N,N-dimethyl-1-(4-nitrophenyl)methanamine Property
- Melting point:
- 118-119 °C
- Boiling point:
- 146-148 °C(Press: 18 Torr)
- Density
- 1.141±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 7.93±0.28(Predicted)
- Appearance
- Light yellow to brown Liquid
Safety
- HS Code
- 2921490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D480518
- Product name
- N,N-Dimethyl-4-nitrobenzylamine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 7197AJ
- Product name
- N,N-Dimethyl-4-nitrobenzylamine
- Packaging
- 1g
- Price
- $89
- Updated
- 2021/12/16
- Product number
- 126967
- Product name
- N,N-Dimethyl-1-(4-nitrophenyl)methanamine
- Purity
- >95%
- Packaging
- 1g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- OR929714
- Product name
- N,N-Dimethyl-4-nitrobenzylamine
- Purity
- 98%
- Packaging
- 1g
- Price
- $131
- Updated
- 2021/12/16
- Product number
- OR929714
- Product name
- N,N-Dimethyl-4-nitrobenzylamine
- Purity
- 98%
- Packaging
- 5g
- Price
- $261
- Updated
- 2021/12/16
N,N-dimethyl-1-(4-nitrophenyl)methanamine Chemical Properties,Usage,Production
Synthesis Reference(s)
The Journal of Organic Chemistry, 38, p. 912, 1973 DOI: 10.1021/jo00945a015
Synthetic Communications, 12, p. 801, 1982 DOI: 10.1080/00397918208061920
Synthesis
124-40-3
100-11-8
15184-96-0
To a solution of 4-nitrobenzyl bromide (10.8 g, 0.05 mol) in acetonitrile (50 mL) was added an excess of dimethylamine (50 mL) and stirred at room temperature for 3 hours. Upon completion of the reaction, water (100 mL) was added to dilute the reaction mixture, which was subsequently extracted twice with dichloromethane (CH2Cl2, 2 x 50 mL). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the target product N,N-dimethyl-4-nitrobenzylamine.
References
[1] Medicinal Chemistry, 2016, vol. 12, # 5, p. 489 - 498
[2] European Journal of Medicinal Chemistry, 2014, vol. 86, p. 257 - 269
[3] Archiv der Pharmazie, 2014, vol. 347, # 12, p. 936 - 949
[4] Patent: WO2006/123145, 2006, A1. Location in patent: Page/Page column 58
[5] Journal of the American Chemical Society, 1983, vol. 105, # 13, p. 4136 - 4142
N,N-dimethyl-1-(4-nitrophenyl)methanamine Preparation Products And Raw materials
Raw materials
Preparation Products
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