ChemicalBook > CAS DataBase List > 5-BROMO-7-CHLORO-1H-INDAZOLE

5-BROMO-7-CHLORO-1H-INDAZOLE

Product Name
5-BROMO-7-CHLORO-1H-INDAZOLE
CAS No.
635712-44-6
Chemical Name
5-BROMO-7-CHLORO-1H-INDAZOLE
Synonyms
5-BROMO-7-CHLORO-1H-INDAZOLE;1H-Indazole, 5-bromo-7-chloro-
CBNumber
CB71501743
Molecular Formula
C7H4BrClN2
Formula Weight
231.48
MOL File
635712-44-6.mol
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5-BROMO-7-CHLORO-1H-INDAZOLE Property

Melting point:
ca 205℃
Boiling point:
364.1℃ @760mmHg
Density 
1.878
storage temp. 
Sealed in dry,Room Temperature
pka
10.67±0.40(Predicted)
Appearance
White to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B689133
Product name
5-Bromo-7-chloro-1h-indazole
Packaging
50mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB42903
Product name
5-Bromo-7-chloro-1H-indazole
Packaging
250mg
Price
$215
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB42903
Product name
5-Bromo-7-chloro-1H-indazole
Packaging
1g
Price
$500
Updated
2021/12/16
Matrix Scientific
Product number
070178
Product name
5-Bromo-7-chloro-1H-indazole
Purity
97%
Packaging
1g
Price
$605
Updated
2021/12/16
Medical Isotopes, Inc.
Product number
37969
Product name
5-Bromo-7-chloro-1H-indazole
Purity
97%
Packaging
1g
Price
$650
Updated
2021/12/16
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5-BROMO-7-CHLORO-1H-INDAZOLE Chemical Properties,Usage,Production

Synthesis

943145-70-8

635712-44-6

In a flame-dried round-bottomed flask, 4-bromo-2-chloro-6-methylphenyl diaza-tert-butyl sulfide (4.60 g, 14.4 mmol) was mixed with potassium tert-butanol (16.1 g, 10 equiv). A stirrer was added and operated under nitrogen atmosphere. Subsequently, anhydrous DMSO (50 mL) was added. The reaction mixture was stirred vigorously for 10 minutes at room temperature. Upon completion of the reaction, the mixture was carefully poured into a mixture consisting of crushed ice (150 mL) and 10% hydrochloric acid (74 mL). The resulting suspension was allowed to stand at 4 °C overnight, after which the solid product was collected by filtration and washed with distilled water. After vacuum drying, 2.86 g of beige solid product (86% yield) was obtained. The product was characterized by 1H-NMR (CDCl3, 500 MHz): δ 7.52 (d, J = 1.5 Hz, 1H), 7.82 (d, J = 1.5 Hz, 1H), 8.08 (s, 1H). Mass spectrometry analysis showed a molecular ion peak (MH+) of 230.90.

References

[1] Patent: WO2003/104236, 2003, A1. Location in patent: Page 122

5-BROMO-7-CHLORO-1H-INDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BROMO-7-CHLORO-1H-INDAZOLE Suppliers

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View Lastest Price from 5-BROMO-7-CHLORO-1H-INDAZOLE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
5-Bromo-7-chloro-1H-indazole 635712-44-6
Price
US $3.00-9.00/KG
Min. Order
0.1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2025-06-26
Career Henan Chemical Co
Product
5-BROMO-7-CHLORO-1H-INDAZOLE 635712-44-6
Price
US $8.80/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
100kg
Release date
2019-07-04

635712-44-6, 5-BROMO-7-CHLORO-1H-INDAZOLERelated Search:


  • 5-BROMO-7-CHLORO-1H-INDAZOLE
  • 1H-Indazole, 5-bromo-7-chloro-
  • 635712-44-6