ChemicalBook > CAS DataBase List > ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride
- Product Name
- ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride
- CAS No.
- 175406-94-7
- Chemical Name
- ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride
- Synonyms
- Methyl 1-benzyl-3-oxo-4-piperidinecarboxylate;Methyl 1-benzyl-3-oxopiperidine-4-carboxylate;Methyl 3-oxo-1-(phenylmethyl)-4-piperidinecarboxylate;ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride;4-Piperidinecarboxylic acid, 3-oxo-1-(phenylmethyl)-, methyl ester
- CBNumber
- CB71522933
- Molecular Formula
- C14H17NO3
- Formula Weight
- 247.29
- MOL File
- 175406-94-7.mol
More
Less
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride Property
- Boiling point:
- 354.4±42.0 °C(Predicted)
- Density
- 1.177±0.06 g/cm3(Predicted)
- pka
- 10.83±0.20(Predicted)
More
Less
N-Bromosuccinimide Price
Crysdot
- Product number
- CD11231725
- Product name
- Methyl1-benzyl-3-oxopiperidine-4-carboxylate
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $79
- Updated
- 2021/12/16
Ambeed
- Product number
- A245104
- Product name
- Methyl1-benzyl-3-oxopiperidine-4-carboxylate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $85
- Updated
- 2021/12/16
Chemenu
- Product number
- CM133177
- Product name
- methyl1-benzyl-3-oxopiperidine-4-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
Alichem
- Product number
- 175406947
- Product name
- Methyl1-benzyl-3-oxopiperidine-4-carboxylate
- Packaging
- 1g
- Price
- $197.96
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11231725
- Product name
- Methyl1-benzyl-3-oxopiperidine-4-carboxylate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $240
- Updated
- 2021/12/16
More
Less
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride Chemical Properties,Usage,Production
Synthesis
40114-49-6
616-38-6
175406-94-7
To a stirred mixture of 1-benzyl-3-piperidone (72 g) and dimethyl carbonate (500 mL) was added sodium hydride (38 g, 60% oil dispersion) in batches. The reaction mixture was heated to reflux for 20 min and then the reaction was quenched by the slow addition of water (800 mL). The aqueous phase was extracted with ethyl acetate (3 x 400 mL), the organic phases were combined and dried over anhydrous sodium sulfate. The organic phase was concentrated under reduced pressure to give methyl 1-benzyl-3-oxopiperidine-4-carboxylate as a brown oil (93 g, 99% yield). lc-MS (ESI+): m/z 248 [M+H]+.
References
[1] Patent: WO2009/26241, 2009, A1. Location in patent: Page/Page column 77-78
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride Suppliers
- Tel
- --
- Fax
- --
- y.barysheva@ukrorgsynth.com
- Country
- Ukraine
- ProdList
- 6230
- Advantage
- 38