2-Bromo-3'-(trifluoromethyl)acetanilide

Product Name: 2-Bromo-3'-(trifluoromethyl)acetanilide
CAS No.: 25625-57-4
Chemical Name: 2-Bromo-3'-(trifluoromethyl)acetanilide
Synonyms: 2-Bromo-N-(3-(trifluoromethyl);2-Bromo-3'-(trifluoromethyl)acetanilide;2-Bromo-3'-(trifluoromethyl)acetanilide 98%;2-bromo-N-[3-(trifluoromethyl)phenyl]ethanamide;2(3H)-Benzoxazolone,6-bromo-5-(triphenylmethyl)-
CBNumber: CB71563811
Molecular Formula: C9H7BrF3NO
Formula Weight: 282.06
MOL File: 25625-57-4.mol

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2-Bromo-3'-(trifluoromethyl)acetanilide Property

Boiling point:: 339.6±42.0 °C(Predicted)
Density: 1.666±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 11.98±0.70(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H228Flammable solid
Precautionary statements: P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB89698
Product name: 2-Bromo-N-[3-(Trifluoromethyl)Phenyl]Acetamide
Packaging: 1g
Price: $170
Updated: 2021/12/16

Matrix Scientific

Product number: 035048
Product name: 2-Bromo-N-[3-(trifluoromethyl)phenyl]acetamide
Packaging: 500mg
Price: $199
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB89698
Product name: 2-Bromo-N-[3-(Trifluoromethyl)Phenyl]Acetamide
Packaging: 2g
Price: $289
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4848-B-02
Product name: 2-Bromo-N-[3-(trifluoromethyl)phenyl]acetamide
Purity: 97%
Packaging: 1g
Price: $395
Updated: 2021/12/16

AK Scientific

Product number: 8499AD
Product name: 2-Bromo-N-[3-(trifluoromethyl)phenyl]acetamide
Packaging: 2g
Price: $440
Updated: 2021/12/16

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2-Bromo-3'-(trifluoromethyl)acetanilide Chemical Properties,Usage,Production

Synthesis

98-16-8

598-21-0

25625-57-4

1. 3-(Trifluoromethyl)aniline (2.0 g, 0.012 mol) was dissolved in dichloromethane (60 ml) under argon protection with stirring. 2. Bromoacetyl bromide (1.2 ml, 0.0137 mol) was slowly added dropwise to the above solution over a period of 10 min, during which the formation of a white precipitate was observed. 3. the reaction mixture was slowly warmed to room temperature and stirring was continued for 1.5 hours. 4. Solid sodium bicarbonate (1.65 g, 0.0196 mol) was added and stirring was continued for 40 minutes. 5. The reaction mixture was treated with water (100 ml), stirred for 10 minutes and then the dichloromethane layer was separated by a phase separation column. 6. The separated methylene chloride layer was concentrated under vacuum to give 2-bromo-N-(3-(trifluoromethyl)phenyl)acetamide as a colorless oil (3.65 g, 100% yield). 7. The product was analyzed by mass spectrometry (ESI). 7. The product was confirmed by mass spectrometry (electrospray LC/MS): the measured value of 282 (MH+) was consistent with the theoretical value of C9H7BrF3NO (281). Retention time 2.74 min. 8. 1H NMR (CDCl3; 400 MHz) data: δ 4.05 (2H, s), 7.40-7.53 (2H, m), 7.76 (1H, d), 7.83 (1H, s), 8.24 (1H, br s).

References

[1] Patent: WO2008/92872, 2008, A1. Location in patent: Page/Page column 40
[2] Patent: WO2008/92877, 2008, A2. Location in patent: Page/Page column 36-37
[3] Patent: WO2008/92878, 2008, A1. Location in patent: Page/Page column 41-42
[4] Patent: WO2009/34062, 2009, A1. Location in patent: Page/Page column 29-30
[5] European Journal of Medicinal Chemistry, 2014, vol. 86, p. 420 - 437

2-Bromo-3'-(trifluoromethyl)acetanilide Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Bromo-3'-(trifluoromethyl)acetanilide Suppliers

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