4-HYDROXY-2-NITRO-ANISOLE

Product Name: 4-HYDROXY-2-NITRO-ANISOLE
CAS No.: 15174-02-4
Chemical Name: 4-HYDROXY-2-NITRO-ANISOLE
Synonyms: 4-METHOXY-3-NITRO-PHENOL;4-HYDROXY-2-NITRO-ANISOLE;Phenol,4-Methoxy-3-nitro-;4-HYDROXY-2-NITRO-ANISOLE ISO 9001：2015 REACH;4-Methoxy-3-nitrophenol@100 μg/mL in Methanol;4-METHOXY-3-NITRO-PHENOL (4-HYDROXY-2-NITRO-ANISOLE)
CBNumber: CB7190555
Molecular Formula: C7H7NO4
Formula Weight: 169.13
MOL File: 15174-02-4.mol

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4-HYDROXY-2-NITRO-ANISOLE Property

Boiling point:: 340.5±27.0 °C(Predicted)
Density: 1.367±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly, Heated, Sonicated)
pka: 8.67±0.10(Predicted)
form: Solid
color: Light Brown to Dark Beige

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Safety

HS Code: 2909500090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M265888
Product name: 4-Methoxy-3-nitrophenol
Packaging: 500mg
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: J93527
Product name: 4-Hydroxy-2-nitroanisole
Packaging: 250mg
Price: $40
Updated: 2021/12/16

ChemScene

Product number: CS-0061910
Product name: 4-Methoxy-3-nitrophenol
Purity: 99.47%
Packaging: 1g
Price: $63
Updated: 2021/12/16

ChemScene

Product number: CS-0061910
Product name: 4-Methoxy-3-nitrophenol
Purity: 99.47%
Packaging: 5g
Price: $185
Updated: 2021/12/16

AK Scientific

Product number: J93527
Product name: 4-Hydroxy-2-nitroanisole
Packaging: 5g
Price: $300
Updated: 2021/12/16

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4-HYDROXY-2-NITRO-ANISOLE Chemical Properties,Usage,Production

Synthesis

39653-87-7

15174-02-4

4-Methoxy-3-nitrophenyl acetate (1.06 g, 5 mmol) was dissolved in ethanol (20 mL) at 0 °C and 1N aqueous sodium hydroxide solution (5.5 mL) was slowly added. The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the reaction was quenched with acetic acid and subsequently extracted twice with ethyl acetate. The organic layers were combined, washed sequentially with water and saturated saline, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford the crude product 4-hydroxy-2-nitroanisole (840 mg, quantitative yield). Thin layer chromatography (TLC) showed an Rf value of 0.59 (ethyl acetate: hexane= 3:7). NMR hydrogen spectrum (400 MHz, CDCl3) data were as follows: δ 3.91 (s, 3H), 6.99 (d, 1H, J = 9.04Hz), 7.17 (dd, 1H, J = 9.04,3.00Hz), 7.38 (d, 1H, J = 3.04Hz).

References

[1] Patent: WO2004/80980, 2004, A1. Location in patent: Page 136
[2] Patent: WO2016/91845, 2016, A1. Location in patent: Page/Page column 83
[3] Monatshefte fuer Chemie, 1914, vol. 35, p. 95
[4] Patent: WO2006/44823, 2006, A2. Location in patent: Page/Page column 165

4-HYDROXY-2-NITRO-ANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-HYDROXY-2-NITRO-ANISOLE Suppliers

China 74 India 1 United Kingdom 2 United States 10 Global 87

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View Lastest Price from 4-HYDROXY-2-NITRO-ANISOLE manufacturers

Career Henan Chemical Co

Product: 4-HYDROXY-2-NITRO-ANISOLE 15174-02-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-25

15174-02-4, 4-HYDROXY-2-NITRO-ANISOLERelated Search:

4-Hydroxy-3-nitrobenzaldehyde 4-(2,5-Diethoxy-4-nitrophenyl)morpholine 2,5-Dimethoxy-4-nitroaniline 1,4-DIMETHOXY-2-NITROBENZENE 1,4-DIBENZYLOXY-2-NITROBENZENE 1,4-DIBUTOXY-2-CHLORO-5-NITROBENZENE 1,4-DIETHOXY-2-NITROBENZENE 1-Chloro-2,5-dimethoxy-4-nitrobenzene 1-CHLORO-2,5-DIETHOXY-4-NITROBENZENE 2,5-DIMETHOXY-3-NITROBENZOIC ACID 2,5-Diethoxy-4-((4-methylphenyl)thio)nitrobenzene 4-(2,5-dibutoxy-4-nitrophenyl)morpholine 4-HYDROXY-2-NITRO-ANISOLE 2,5-dimethoxy-4-nitrobenzonitrile 3,6-DIMETHOXY-2-NITROBENZALDEHYDE 2-[(2,5-DIMETHOXY-4-NITROPHENYL)THIO]ETHANOHYDRAZIDE 1-CHLORO-5-ETHOXY-4-NITRO-2-PROPOXYBENZENE 1-BUTOXY-5-CHLORO-4-ETHOXY-2-NITROBENZENE

4-HYDROXY-2-NITRO-ANISOLE

4-METHOXY-3-NITRO-PHENOL

4-METHOXY-3-NITRO-PHENOL (4-HYDROXY-2-NITRO-ANISOLE)

Phenol,4-Methoxy-3-nitro-

4-Methoxy-3-nitrophenol@100 μg/mL in Methanol

4-HYDROXY-2-NITRO-ANISOLE ISO 9001：2015 REACH

15174-02-4