3-IODO-7-METHYL (1H)INDAZOLE
- Product Name
- 3-IODO-7-METHYL (1H)INDAZOLE
- CAS No.
- 847906-27-8
- Chemical Name
- 3-IODO-7-METHYL (1H)INDAZOLE
- Synonyms
- 3-IODO-7-METHYLINDAZOLE;3-iodo-7-methyl-2H-indazole;1H-Indazole,3-iodo-7-Methyl-;3-IODO-7-METHYL (1H)INDAZOLE
- CBNumber
- CB7193682
- Molecular Formula
- C8H7IN2
- Formula Weight
- 258.06
- MOL File
- 847906-27-8.mol
3-IODO-7-METHYL (1H)INDAZOLE Property
- Boiling point:
- 368.6±22.0 °C(Predicted)
- Density
- 1.933±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 12.43±0.40(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- Y4209
- Product name
- 3-Iodo-7-methyl-1H-indazole
- Packaging
- 100mg
- Price
- $178
- Updated
- 2021/12/16
- Product number
- HCH0063541
- Product name
- 3-IODO-7-METHYL (1H)INDAZOLE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.68
- Updated
- 2021/12/16
- Product number
- Y4209
- Product name
- 3-Iodo-7-methyl-1H-indazole
- Packaging
- 1g
- Price
- $521
- Updated
- 2021/12/16
- Product number
- BB20-7218B
- Product name
- 3-Iodo-7-methyl-2H-indazole
- Purity
- 95%
- Packaging
- 5G
- Price
- $895
- Updated
- 2021/12/16
- Product number
- A150309
- Product name
- 3-Iodo-7-methyl-1H-indazole
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1155
- Updated
- 2021/12/16
3-IODO-7-METHYL (1H)INDAZOLE Chemical Properties,Usage,Production
Synthesis
3176-66-7
847906-27-8
7-Methyl-1H-indazole (2 g, 15.15 mmol) was added potassium hydroxide (KOH, 2.12 g, 37.88 mmol) and iodine (I2, 7.7 g, 30.3 mmol) in N,N-dimethylformamide (DMF, 40 mL) and the reaction was stirred at room temperature for 4 hours. After completion of the reaction, the mixture was poured into water (200 mL) and extracted with ethyl acetate (EA, 200 mL). The organic layer was washed sequentially with saturated sodium sulfite solution (100 mL), water (200 mL) and saturated brine (200 mL), dried over anhydrous sodium sulfate (Na2SO4), and concentrated under reduced pressure to afford the target product 3-iodo-7-methyl-1H-indazole (3.6 g, 92% yield) as a yellow solid.
References
[1] Patent: WO2018/132372, 2018, A1. Location in patent: Paragraph 01237
[2] Patent: US2005/54697, 2005, A1. Location in patent: Page/Page column 73
3-IODO-7-METHYL (1H)INDAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-IODO-7-METHYL (1H)INDAZOLE manufacturers
- Product
- 3-IODO-7-METHYL (1H)INDAZOLE 847906-27-8
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02