Uses
ChemicalBook > CAS DataBase List > 2,6-Dichloronicotinamide

2,6-Dichloronicotinamide

Uses
Product Name
2,6-Dichloronicotinamide
CAS No.
62068-78-4
Chemical Name
2,6-Dichloronicotinamide
Synonyms
DichloronicotinaMide;2,6-Dichloronicotimide;Nicotinamide Impurity 99;2,6-Dichloronicotinamide;2,6-Dichloropyridine-3-carboxamide;3-Pyridinecarboxamide, 2,6-dichloro-;2,6-Dichloropyridine-3-carboxamide 97%;2,6-Dichloronicotinamide ISO 9001：2015 REACH
CBNumber
CB72100659
Molecular Formula
C6H4Cl2N2O
Formula Weight
191.01
MOL File
62068-78-4.mol
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2,6-Dichloronicotinamide Property

Melting point:
148-151 °C
Boiling point:
315.5±42.0 °C(Predicted)
Density 
1.524±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
powder
pka
13.91±0.50(Predicted)
Appearance
White to off-white Solid
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Safety

Hazard Codes 
Xn
Risk Statements 
22-36/37/38
Safety Statements 
26
WGK Germany 
3
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
702145
Product name
2,6-Dichloropyridine-3-carboxamide
Purity
97%
Packaging
5g
Price
$334
Updated
2023/06/20
Sigma-Aldrich
Product number
702145
Product name
2,6-Dichloropyridine-3-carboxamide
Purity
97%
Packaging
1g
Price
$76
Updated
2023/01/07
TRC
Product number
D435738
Product name
2,6-Dichloronicotinamide
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
D435738
Product name
2,6-Dichloronicotinamide
Packaging
50mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
J96732
Product name
2,6-Dichloronicotinamide
Packaging
250mg
Price
$24
Updated
2021/12/16
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2,6-Dichloronicotinamide Chemical Properties,Usage,Production

Uses

2,6-Dichloronicotinamide is used as a research compound and in organic synthesis, etc.

Synthesis

40381-90-6

62068-78-4

General procedure for the synthesis of 2,6-dichloronicotinamide from 2,6-dichloronicotinonitrile: To 2,6-dichloronicotinonitrile (1.73 g, 10 mmol) was added concentrated sulfuric acid (10 mL) and water (2 mL). The reaction mixture was heated to 90 °C and stirred continuously for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently slowly poured into ice water. The pH of the mixture was adjusted with ammonia to 8. The precipitate precipitated was collected by filtration, washed with cold water (20 mL) and finally dried under vacuum to give 2,6-dichloronicotinamide as a brown solid (1.4 g, 73% yield). Mass spectrum (ESI): m/z = 191.1 [M + H]+.

References

[1] Patent: WO2015/48662, 2015, A2. Location in patent: Page/Page column 37
[2] Patent: CN107226805, 2017, A. Location in patent: Paragraph 0097; 0098; 0099; 0100; 0101

2,6-Dichloronicotinamide Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-Dichloronicotinamide Suppliers

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View Lastest Price from 2,6-Dichloronicotinamide manufacturers

Career Henan Chemical Co
Product
2,6-Dichloronicotinamide 62068-78-4
Price
US $1.00/kg
Min. Order
1g
Purity
99%
Supply Ability
100KG
Release date
2018-12-21

62068-78-4, 2,6-DichloronicotinamideRelated Search:

2,6-DICHLORO(3-PYRIDYL) 4-(5-(TRIFLUOROMETHYL)(2-PYRIDYL))PIPERAZINYL KETONE 2,6-DICHLORO-4-(TRIFLUOROMETHYL)NICOTINAMIDE 2,6-DICHLORO-4-METHYLNICOTINAMIDE N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(2,5-DICHLOROPHENYL)UREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(3,4-DICHLOROPHENYL)UREA 1-[4-(4-CHLOROPHENOXY)PHENYL]-3-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]IMIDAZOLIDINE-2,4,5-TRIONE N-[4-(4-CHLOROPHENOXY)PHENYL]-N'-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]UREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(3,5-DICHLOROPHENYL)UREA N-(4-CHLOROPHENYL)-N'-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]UREA 2,6-DICHLORO(3-PYRIDYL)4-(3-CHLORO-5-(TRIFLUOROMETHYL)(2-PYRIDYL))PIPERAZINYL KETONE N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-PIPERIDINOUREA (2,6-DICHLORO(3-PYRIDYL))-N-(4-(3-CHLORO-5-(TRIFLUOROMETHYL)(2-PYRIDYLTHIO))PHENYL)FORMAMIDE (2,6-DICHLORO-4-METHYLPYRIDIN-3-YL)([(([(2,6-DICHLOROPHENYL)METHYLENE]AMINO)OXY)CARBONYL]AMINO)METHANONE N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(2,4-DICHLOROPHENYL)UREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(2,6-DICHLOROPHENYL)UREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(4H-1,2,4-TRIAZOL-4-YL)UREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-MORPHOLINOUREA N-[(2,6-DICHLORO-4-METHYL-3-PYRIDYL)CARBONYL]-N'-(2,3-DICHLOROPHENYL)UREA

  • 2,6-Dichloronicotinamide
  • 2,6-Dichloropyridine-3-carboxamide
  • DichloronicotinaMide
  • 2,6-Dichloronicotimide
  • 2,6-Dichloropyridine-3-carboxamide 97%
  • 3-Pyridinecarboxamide, 2,6-dichloro-
  • 2,6-Dichloronicotinamide ISO 9001：2015 REACH
  • Nicotinamide Impurity 99
  • 62068-78-4