ChemicalBook > CAS DataBase List > 3,4,5-TRIFLUOROIODOBENZENE

3,4,5-TRIFLUOROIODOBENZENE

Product Name: 3,4,5-TRIFLUOROIODOBENZENE
CAS No.: 170112-66-0
Chemical Name: 3,4,5-TRIFLUOROIODOBENZENE
Synonyms: SKL330;3,4,5-TRIFLUOROIODOBENZENE;1-Iodo-3,4,5-Trifluorobenzene;5-Iodo-1,2,3-trifluorobenzene;1,2,3-trifluoro-5-iodobenzene;Benzene, 1,2,3-trifluoro-5-iodo-
CBNumber: CB7235915
Molecular Formula: C6H2F3I
Formula Weight: 257.98
MOL File: 170112-66-0.mol

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3,4,5-TRIFLUOROIODOBENZENE Property

Boiling point:: 176.4±35.0 °C(Predicted)
Density: 2.078±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: liquid
color: Clear, pale peach

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
HazardClass: IRRITANT
HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: T895658
Product name: 3,4,5-Trifluoroiodobenzene
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 012627
Product name: 3,4,5-Trifluoroiodobenzene
Purity: 98%
Packaging: 5g
Price: $52
Updated: 2021/12/16

Apolloscientific

Product number: PC2701
Product name: 3,4,5-Trifluoroiodobenzene
Packaging: 5g
Price: $70
Updated: 2021/12/16

Apolloscientific

Product number: PC2701
Product name: 3,4,5-Trifluoroiodobenzene
Packaging: 1g
Price: $19
Updated: 2021/12/16

Matrix Scientific

Product number: 012627
Product name: 3,4,5-Trifluoroiodobenzene
Purity: 98%
Packaging: 1g
Price: $19
Updated: 2021/12/16

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3,4,5-TRIFLUOROIODOBENZENE Chemical Properties,Usage,Production

Synthesis

138526-69-9

170112-66-0

The general procedure for the synthesis of 3,4,5-trifluoroiodobenzene from 3,4,5-trifluorobromobenzene was as follows: first, magnesium (5.76 g, 237 mmol) and iodine (10.0 mg, 40.0 μmol) were added to tetrahydrofuran (190 mL), followed by the slow dropwise addition of 3,4,5-trifluorobromobenzene (50.0 g, 237 mmol). The reaction mixture was stirred at room temperature for 30 min. Next, a tetrahydrofuran solution (160 mL) of iodine (66.1 g, 261 mmol) was added at 0 °C and the mixture was continued to be stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was poured into ice water, neutralized with concentrated hydrochloric acid and then extracted with hexane. The extract was sequentially washed with saturated aqueous sodium thiosulfate and dried over anhydrous sodium sulfate, followed by concentration under reduced pressure. Finally, the concentrate was purified by silica gel column chromatography (eluent: ethyl acetate/hexane=1/10) to afford the title compound 3,4,5-trifluoroiodobenzene as a yellow oil (yield 45.0 g, 70%).1H NMR (CDCl3) δ: 7.32 (2H, t, J=6.4 Hz).

References

[1] Patent: JP2016/84346, 2016, A. Location in patent: Paragraph 0050
[2] Patent: JP2016/84328, 2016, A. Location in patent: Paragraph 0187
[3] Patent: JP2016/84347, 2016, A. Location in patent: Paragraph 0136
[4] Patent: JP2016/84348, 2016, A. Location in patent: Paragraph 0064
[5] Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002, vol. 373, p. 17 - 24

3,4,5-TRIFLUOROIODOBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,4,5-TRIFLUOROIODOBENZENE manufacturers

Career Henan Chemical Co

Product: 3,4,5-TRIFLUOROIODOBENZENE 170112-66-0
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

170112-66-0, 3,4,5-TRIFLUOROIODOBENZENERelated Search:

Trifluoromethanesulfonic acid Chromium(VI) oxide 3,4,5-TRIFLUOROIODOBENZENE, 97 2,3,5-Trifluoroiodobenzene 2,3,4-TRIFLUOROIODOBENZENE 2,4,6-TRIFLUOROIODOBENZENE 2,4,5-TRIFLUOROIODOBENZENE 2,3,4-TRIFLUOROIODOBENZENE 97 2,4,5-TRIFLUOROIODOBENZENE 97% 2-BROMO-3,4,5-TRIFLUOROIODOBENZENE 3,4,5-TRIFLUOROIODOBENZENE IODOPENTAFLUOROBENZENE 1,2-DIIODOTETRAFLUOROBENZENE [BIS(TRIFLUOROACETOXY)IODO]PENTAFLUOROBENZENE

3,4,5-TRIFLUOROIODOBENZENE

1,2,3-trifluoro-5-iodobenzene

5-Iodo-1,2,3-trifluorobenzene

1-Iodo-3,4,5-Trifluorobenzene

Benzene, 1,2,3-trifluoro-5-iodo-

SKL330

170112-66-0