ChemicalBook > CAS DataBase List > 5-PHENYL-1H-IMIDAZOL-2-AMINE

5-PHENYL-1H-IMIDAZOL-2-AMINE

Product Name: 5-PHENYL-1H-IMIDAZOL-2-AMINE
CAS No.: 6775-40-2
Chemical Name: 5-PHENYL-1H-IMIDAZOL-2-AMINE
Synonyms: 4-phenyl-1H-imidazol-2-amine;2-Amino-5-phenylimidazole;4-Phenylimidazole-2-amine;5-PHENYL-1H-IMIDAZOL-2-AMINE;1H-Imidazol-2-amine, 5-phenyl-;4-Phenyl-1H-imidazol-2-ylamine;5-Phenyl-1H-iMidazol-2-ylaMine;1H-IMidazol-2-aMine, 4-phenyl-;2-aMino-1H-4(5)-phenyliMidazole
CBNumber: CB72448593
Molecular Formula: C9H9N3
Formula Weight: 159.19
MOL File: 6775-40-2.mol

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5-PHENYL-1H-IMIDAZOL-2-AMINE Property

Melting point:: 245 °C(Solv: ethanol (64-17-5))
Boiling point:: 421.3±38.0 °C(Predicted)
Density: 1.238±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 14.75±0.10(Predicted)
Appearance: Yellow to brown Solid
InChI: InChI=1S/C9H9N3/c10-9-11-6-8(12-9)7-4-2-1-3-5-7/h1-6H,(H3,10,11,12)
InChIKey: NODFMZCEEBQXME-UHFFFAOYSA-N
SMILES: C1(N)NC(C2=CC=CC=C2)=CN=1

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Safety

Hazard Codes: Xn
Risk Statements: 22-36/38
Safety Statements: 26
WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P677540
Product name: 5-Phenyl-1H-imidazol-2-amine
Packaging: 50mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 0440AC
Product name: 5-Phenyl-1H-imidazol-2-amine
Packaging: 250mg
Price: $213
Updated: 2021/12/16

Matrix Scientific

Product number: 089736
Product name: 5-Phenyl-1H-imidazol-2-amine
Purity: 95+%
Packaging: 250mg
Price: $394
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0376560
Product name: 5-PHENYL-1H-IMIDAZOL-2-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $502.74
Updated: 2021/12/16

Matrix Scientific

Product number: 089736
Product name: 5-Phenyl-1H-imidazol-2-amine
Purity: 95+%
Packaging: 1g
Price: $874
Updated: 2021/12/16

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5-PHENYL-1H-IMIDAZOL-2-AMINE Chemical Properties,Usage,Production

Synthesis

160041-64-5

6775-40-2

Compound 17 (500 mg) was taken as raw material and mixed with 6M hydrochloric acid (2.2 mL) and methanol (2.5 mL) and reacted at reflux for 3 hours. After completion of the reaction, the mixture was cooled to room temperature and the precipitate was collected by filtration. The filtrate was concentrated under vacuum and the residue was dissolved in water and neutralized with 1 M sodium hydroxide solution. A precipitate was precipitated from the neutralized solution, collected by vacuum filtration and washed sequentially with water and ether to afford the target product 5-phenyl-1H-imidazol-2-amine (18, 131 mg, 33% yield) as a light brown solid. The product was characterized by 1H NMR (DMSO-d6): δ 5.25 (2H, s), 6.96 (1H, s), 7.07 (1H, t, J = 7.5 Hz), 7.26 (2H, t, J = 7.5 Hz), 7.57 (2H, d, J = 7.5 Hz), 10.53 (1H, br s). Mass spectrometry analysis showed FAB MS m/e (M + H)+ 160; high-resolution mass spectrometry (ESI) measured 160.0875 calculated and 160.0871 measured values for C9H10N3 (M + H)+. Elemental analyses of the calculated values (C9H9N3-3H2O): C, 65.68; H, 5.88; N, 25.53; measured values: C. 65.81; H, 5.49; N, 25.19.

References

[1] Journal of Medicinal Chemistry, 2018, vol. 61, # 7, p. 2806 - 2822
[2] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 13, p. 3873 - 3881
[3] Journal of Heterocyclic Chemistry, 2017, vol. 54, # 1, p. 524 - 530
[4] Journal of Heterocyclic Chemistry, 2018, vol. 55, # 6, p. 1410 - 1418

5-PHENYL-1H-IMIDAZOL-2-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6775-40-2, 5-PHENYL-1H-IMIDAZOL-2-AMINERelated Search:

2-(4-BROMO-PHENYL)-7-METHYL-IMIDAZO[1,2-A]PYRIMIDINE 2-(4-NITRO-PHENYL)-IMIDAZO[1,2-A]PYRIMIDINE 2-(3,4-DICHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE 2-PHENYLIMIDAZO[1,2-A]PYRIMIDINE 4,5-DIPHENYL-IMIDAZOLE-1,2-DIAMINE 4-(4-BROMOPHENYL)-N1-[(E)-PHENYLMETHYLIDENE]-1H-IMIDAZOLE-1,2-DIAMINE 8-METHYL-2-PHENYL-8H-1,3A,8-TRIAZA-CYCLOPENTA[A]INDENE-3-CARBALDEHYDE 1-AMINO-4-(4-CHLOROPHENYL)-1H-IMIDAZOL-2-YLAMINE 1-methyl-4-p-tolyl-1H-imidazol-2-amine 1-(9-BENZYL-2-PHENYL-9H-IMIDAZO[1,2-A]BENZIMIDAZOL-3-YL)-2,2,2-TRICHLOROETHANONE 4-PHENYL-N1-[(1E)-PHENYLMETHYLENE]-1H-IMIDAZOLE-1,2-DIAMINE 2-(4-CHLOROPHENYL)-9H-IMIDAZO[1,2-A]BENZIMIDAZOL-9-AMINE 4-PHENYL-1H-IMIDAZOLE-1,2-DIAMINE 4-IMIDAZO[1,2-A]PYRIMIDIN-2-YLPHENYL METHYL ETHER 9-BENZYL-2-PHENYL-9H-IMIDAZO[1,2-A]BENZIMIDAZOLE-3-CARBOHYDRAZIDE 3-(8-METHYL-2-PHENYL-8H-1,3A,8-TRIAZA-CYCLOPENTA[A]INDEN-3-YL)-PROPIONIC ACID 8-METHYL-2-PHENYL-8H-1,3A,8-TRIAZA-CYCLOPENTA[A]INDENE 2-(4-CHLOROPHENYL)IMIDAZO[1,2-A]PYRIMIDINE

5-PHENYL-1H-IMIDAZOL-2-AMINE

1H-IMidazol-2-aMine, 4-phenyl-

5-Phenyl-1H-iMidazol-2-ylaMine

2-aMino-1H-4(5)-phenyliMidazole

4-phenyl-1H-imidazol-2-amine

4-Phenylimidazole-2-amine

4-Phenyl-1H-imidazol-2-ylamine

1H-Imidazol-2-amine, 5-phenyl-

2-Amino-5-phenylimidazole

6775-40-2