ChemicalBook > CAS DataBase List > DI(1H-IMIDAZOL-1-YL)METHANIMINE

DI(1H-IMIDAZOL-1-YL)METHANIMINE

Product Name: DI(1H-IMIDAZOL-1-YL)METHANIMINE
CAS No.: 104619-51-4
Chemical Name: DI(1H-IMIDAZOL-1-YL)METHANIMINE
Synonyms: EOS-60817;Di(1-iMidazolyl)MethaniMine;Di (1H imidazol-1-yl) imine;di(imidazol-1-yl)methanimine;Di(1H-imidazol-2-yl)methanimine;DI(1H-IMIDAZOL-1-YL)METHANIMINE;Di (1 hydrogen imidazolyl) imine;C,C-di(imidazol-1-yl)methaneimine;1,1'-Carbonimidoylbis-1H-imidazole;1,1'-Carbonimidoylbis[1H-imidazole
CBNumber: CB72454846
Molecular Formula: C7H7N5
Formula Weight: 161.16
MOL File: 104619-51-4.mol

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DI(1H-IMIDAZOL-1-YL)METHANIMINE Property

Melting point:: 103-104℃
Boiling point:: 355℃
Density: 1.38
Flash point:: 169℃
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 4.19±0.70(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C7H7N5/c8-7(11-3-1-9-5-11)12-4-2-10-6-12/h1-6,8H
InChIKey: FKGQRXQOODICAT-UHFFFAOYSA-N
SMILES: C(N1C=NC=C1)(N1C=NC=C1)=N

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Safety

HS Code: 2933299090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: D476993
Product name: Di(1H-imidazol-1-yl)methanimine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC45505
Product name: 1,1'-Carbonimidoylbis-1H-imidazole
Packaging: 2g
Price: $110
Updated: 2021/12/16

Apolloscientific

Product number: OR917034
Product name: 1,1'-Carbonimidoylbis-1H-imidazole
Purity: 95%
Packaging: 1g
Price: $155
Updated: 2021/12/16

ChemScene

Product number: CS-D0450
Product name: 1,1'-Carbonimidoylbis[1H-imidazole]
Packaging: 5g
Price: $184
Updated: 2021/12/16

ChemScene

Product number: CS-D0450
Product name: 1,1'-Carbonimidoylbis[1H-imidazole]
Packaging: 1g
Price: $55
Updated: 2021/12/16

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DI(1H-IMIDAZOL-1-YL)METHANIMINE Chemical Properties,Usage,Production

Synthesis

288-32-4

506-68-3

104619-51-4

Cyanogen bromide (22.5 g, 212 mmol) was slowly added to a solution of 1H-imidazole (42 g, 617 mmol) in dichloromethane (1 L) and the reaction mixture was heated to reflux for 30 min. After completion of the reaction, it was cooled to room temperature and white solid was observed to precipitate. The solid was separated by filtration. The filtrate was concentrated under reduced pressure to about 100 mL and subsequently allowed to stand in a refrigerator for 3 days to promote crystallization. The precipitated solid was collected by filtration to give the final bis(1H-imidazol-1-yl)methanimine (8 g, 49.6 mmol, 8% yield).

References

[1] Patent: US2012/149718, 2012, A1. Location in patent: Page/Page column 35
[2] Journal of Organic Chemistry, 2002, vol. 67, # 21, p. 7553 - 7556
[3] Journal of Heterocyclic Chemistry, 2003, vol. 40, # 1, p. 191 - 193
[4] Chemical Communications, 2014, vol. 50, # 91, p. 14257 - 14260
[5] Patent: WO2012/85586, 2012, A1. Location in patent: Page/Page column 66; 68

DI(1H-IMIDAZOL-1-YL)METHANIMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from DI(1H-IMIDAZOL-1-YL)METHANIMINE manufacturers

Career Henan Chemical Co

Product: DI(1H-IMIDAZOL-1-YL)METHANIMINE 104619-51-4
Price: US $2.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: customise
Release date: 2018-08-09

104619-51-4, DI(1H-IMIDAZOL-1-YL)METHANIMINERelated Search:

DI(1H-IMIDAZOL-1-YL)METHANIMINE

C,C-di(imidazol-1-yl)methaneimine

1,1'-Carbonimidoylbis-1H-imidazole

Di(1-iMidazolyl)MethaniMine

Di(1H-imidazol-2-yl)methanimine

1-(1H-imidazole-1-carboximidoyl)-1H-imidazole

di(imidazol-1-yl)methanimine

EOS-60817

1H-IMidazole, 1,1'-carboniMidoylbis-

C-(Di-iMidazol-1-yl)-MethyleneaMine

1,1-Di(1H-imidazol-1-yl)methanimine

Di (1H imidazol-1-yl) imine

1,1'-Carbonimidoylbis[1H-imidazole

1-(IMIDAZOLE-1-CARBOXIMIDOYL)IMIDAZOLE

Di (1 hydrogen imidazolyl) imine

104619-51-4