1-IODO-2-NITRO-4-CHLOROBENZENE
- Product Name
- 1-IODO-2-NITRO-4-CHLOROBENZENE
- CAS No.
- 5446-05-9
- Chemical Name
- 1-IODO-2-NITRO-4-CHLOROBENZENE
- Synonyms
- NSC 17163;5-Chloro-2-iodonitrobenzene;4-choro-1-iode-2-nitrobenzene;4-Chloro-2-nitrophenyl iodide;1-IODO-2-NITRO-4-CHLOROBENZENE;Benzene, 4-chloro-1-iodo-2-nitro-
- CBNumber
- CB72460472
- Molecular Formula
- C6H3ClINO2
- Formula Weight
- 283.45
- MOL File
- 5446-05-9.mol
1-IODO-2-NITRO-4-CHLOROBENZENE Property
- Melting point:
- 59℃
- Boiling point:
- 297.7±25.0 °C(Predicted)
- Density
- 2.094±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2930.90.4950
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- C2932
- Product name
- 4-Chloro-1-iodo-2-nitrobenzene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $64
- Updated
- 2025/07/31
- Product number
- C2932
- Product name
- 4-Chloro-1-iodo-2-nitrobenzene
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $190
- Updated
- 2025/07/31
- Product number
- C382265
- Product name
- 4-Chloro-1-iodo-2-nitrobenzene
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FC76331
- Product name
- 4-Chloro-1-iodo-2-nitrobenzene
- Packaging
- 1g
- Price
- $68
- Updated
- 2021/12/16
- Product number
- FC76331
- Product name
- 4-Chloro-1-iodo-2-nitrobenzene
- Packaging
- 2g
- Price
- $108.8
- Updated
- 2021/12/16
1-IODO-2-NITRO-4-CHLOROBENZENE Chemical Properties,Usage,Production
Synthesis
6280-88-2
5446-05-9
General procedure for the synthesis of 4-chloro-1-iodo-2-nitrobenzene from 4-chloro-2-nitrobenzoic acid: 6.2 mg of silver sulfate, 21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-phenanthroline, 40.3 mg of 4-chloro-2-nitrobenzoic acid, and 45 mg of iodine were sequentially added to a Silak reaction tube equipped with a magnetic stirrer. The reaction mixture was heated at 160°C for 24 hours under oxygen atmosphere. After completion of the reaction, the reaction was quenched by addition of distilled water and extracted three times with ethyl acetate. The organic phases were combined and concentrated to give 40.8 mg of 4-chloro-1-iodo-2-nitrobenzene in 72% yield.
References
[1] Journal of Organic Chemistry, 2016, vol. 81, # 7, p. 2794 - 2803
[2] Patent: CN107325002, 2017, A. Location in patent: Page/Page column 6; 7
[3] Organic and Biomolecular Chemistry, 2018, vol. 16, # 30, p. 5416 - 5421
1-IODO-2-NITRO-4-CHLOROBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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