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5-BENZYL-1H-PYRAZOL-3-AMINE

Product Name
5-BENZYL-1H-PYRAZOL-3-AMINE
CAS No.
150712-24-6
Chemical Name
5-BENZYL-1H-PYRAZOL-3-AMINE
Synonyms
3-amino-5-benzypyrazole;5-Benzyl-2H-pyrazol-3-amine;5-BENZYL-1H-PYRAZOL-3-AMINE;5-Benzyl-3-amino-1H-pyrazole;5-Benzyl-1H-pyrazol-3-ylamine;1H-Pyrazol-3-amine, 5-(phenylmethyl)-;Acetamide,N-[6-(aminosulfonyl)phenyl]-
CBNumber
CB72464652
Molecular Formula
C10H11N3
Formula Weight
173.21
MOL File
150712-24-6.mol
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5-BENZYL-1H-PYRAZOL-3-AMINE Property

Boiling point:
405.3±30.0 °C(Predicted)
Density 
1.214±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
15.92±0.10(Predicted)
Appearance
Off-white to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B411778
Product name
5-Benzyl-1H-pyrazol-3-amine
Packaging
100mg
Price
$175
Updated
2021/12/16
AK Scientific
Product number
1427DA
Product name
5-Benzyl-1H-pyrazol-3-amine
Packaging
250mg
Price
$445
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0383600
Product name
5-BENZYL-1H-PYRAZOL-3-AMINE
Purity
95.00%
Packaging
5MG
Price
$503.7
Updated
2021/12/16
Ambeed
Product number
A172084
Product name
5-Benzyl-1H-pyrazol-3-amine
Purity
97%
Packaging
100mg
Price
$78
Updated
2021/12/16
Ambeed
Product number
A172084
Product name
5-Benzyl-1H-pyrazol-3-amine
Purity
97%
Packaging
250mg
Price
$113
Updated
2021/12/16
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5-BENZYL-1H-PYRAZOL-3-AMINE Chemical Properties,Usage,Production

Synthesis

19212-27-2

150712-24-6

General procedure for the synthesis of 3-amino-5-benzyl-1H-pyrazole from 3-oxo-4-phenylbutanenitrile: A mixed solution of 3-oxo-4-phenylbutanenitrile (Method 26; 0.58 g, 3.64 mmol) with hydrazine monohydrate (0.177 mL, 3.64 mmol) in ethanol (16 mL) was heated and refluxed for 3 hours. Upon completion of the reaction, the mixture was cooled to 25 °C and subsequently concentrated under reduced pressure. The reaction mixture was extracted with dichloromethane (15 mL) and washed twice with saturated saline. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give an orange solid. The solid was ground with a mixture of hexane and ether (1:1) and collected by filtration to afford 3-amino-5-benzyl-1H-pyrazole as a yellow solid (0.38 g, 60% yield).1H NMR (400 MHz, CDCl3) δ 3.9 (s, 2H), 4.89 (br s, 1H), 5.44 (s, 1H), 7.19-7.34 (m 5H). Mass spectrum (MS): calculated value: 173; measured value: [M + H]+ 174.

References

[1] Patent: WO2005/49033, 2005, A1. Location in patent: Page/Page column 99
[2] Patent: WO2008/62026, 2008, A1. Location in patent: Page/Page column 20

5-BENZYL-1H-PYRAZOL-3-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BENZYL-1H-PYRAZOL-3-AMINE Suppliers

A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 5-BENZYL-1H-PYRAZOL-3-AMINE manufacturers

Career Henan Chemical Co
Product
5-BENZYL-1H-PYRAZOL-3-AMINE 150712-24-6
Price
US $1.00/g
Min. Order
1g
Purity
98%
Supply Ability
100KG
Release date
2020-01-12

150712-24-6, 5-BENZYL-1H-PYRAZOL-3-AMINERelated Search:


  • 5-BENZYL-1H-PYRAZOL-3-AMINE
  • 5-Benzyl-2H-pyrazol-3-amine
  • 5-Benzyl-3-amino-1H-pyrazole
  • 1H-Pyrazol-3-amine, 5-(phenylmethyl)-
  • Acetamide,N-[6-(aminosulfonyl)phenyl]-
  • 5-Benzyl-1H-pyrazol-3-ylamine
  • 3-amino-5-benzypyrazole
  • 150712-24-6