ChemicalBook > CAS DataBase List > Methyl 2,6-dichloro-4-cyanobenzoate

Methyl 2,6-dichloro-4-cyanobenzoate

Product Name: Methyl 2,6-dichloro-4-cyanobenzoate
CAS No.: 409127-32-8
Chemical Name: Methyl 2,6-dichloro-4-cyanobenzoate
Synonyms: 2，6-dichloro-4-cyanobenzoic acid;Methyl 2,6-dichloro-4-cyanobenzoate;Methyl 2,6-difluoro-4-Cyanobenzoate;Benzoic acid, 2,6-dichloro-4-cyano-, methyl ester
CBNumber: CB72470844
Molecular Formula: C9H5Cl2NO2
Formula Weight: 230.05
MOL File: 409127-32-8.mol

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Methyl 2,6-dichloro-4-cyanobenzoate Property

Boiling point:: 319.6±42.0 °C(Predicted)
Density: 1.45
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 097913
Product name: Methyl 2,6-dichloro-4-cyanobenzoate
Purity: 95+%
Packaging: 250mg
Price: $439
Updated: 2021/12/16

Matrix Scientific

Product number: 097913
Product name: Methyl 2,6-dichloro-4-cyanobenzoate
Purity: 95+%
Packaging: 1g
Price: $975
Updated: 2021/12/16

Ambeed

Product number: A487149
Product name: Methyl2,6-dichloro-4-cyanobenzoate
Purity: 98%
Packaging: 100mg
Price: $86
Updated: 2021/12/16

Ambeed

Product number: A487149
Product name: Methyl2,6-dichloro-4-cyanobenzoate
Purity: 98%
Packaging: 250mg
Price: $152
Updated: 2021/12/16

Ambeed

Product number: A487149
Product name: Methyl2,6-dichloro-4-cyanobenzoate
Purity: 98%
Packaging: 1g
Price: $428
Updated: 2021/12/16

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Methyl 2,6-dichloro-4-cyanobenzoate Chemical Properties,Usage,Production

Synthesis

409127-31-7

409127-32-8

Step a: Synthesis of methyl 2,6-dichloro-4-cyanobenzoate Methyl 4-carbamoyl-2,6-dichlorobenzoate (100 mg, 0.4 mmol) was dissolved in pyridine (2 mL) and trifluoroacetic anhydride (0.11 mL, 0.8 mmol) was added slowly and dropwise at 0 °C. The reaction mixture was gradually warmed to room temperature and stirred continuously for 1 hour. Upon completion of the reaction, the mixture was poured into pre-cooled ice water, the precipitated solid was filtered, washed thoroughly with cold water and dried to afford methyl 2,6-dichloro-4-cyanobenzoate (55 mg, 88% yield) as an off-white solid.

References

[1] Patent: WO2012/160464, 2012, A1. Location in patent: Page/Page column 77-78
[2] Patent: US2014/155398, 2014, A1. Location in patent: Paragraph 0468
[3] Patent: US2010/317643, 2010, A1. Location in patent: Page/Page column 101
[4] Journal of Medicinal Chemistry, 2013, vol. 56, # 11, p. 4521 - 4536

Methyl 2,6-dichloro-4-cyanobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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409127-32-8, Methyl 2,6-dichloro-4-cyanobenzoateRelated Search:

Methyl 2,6-dichloro-4-cyanobenzoate

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409127-32-8