ChemicalBook > CAS DataBase List > 1-Bromo-4-iodonaphthalene

1-Bromo-4-iodonaphthalene

Product Name
1-Bromo-4-iodonaphthalene
CAS No.
63279-58-3
Chemical Name
1-Bromo-4-iodonaphthalene
Synonyms
1,4-BIN;1-Bromo-4-iodophthalene;-BroMo-4-iodonaphthalene;1-Iodo-4-bromonaphthalene;1-Bromo-4-iodonaphthalene;4-bromo-1-iodonaphthalene;1-Bromo-4-iodonaphthaIene;1-Bromo-4-Iodine Naphthalene;Naphthalene, 1-bromo-4-iodo-;1-Bromo-4-iodonaphthalene 98%
CBNumber
CB72506879
Molecular Formula
C10H6BrI
Formula Weight
332.96
MOL File
63279-58-3.mol
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1-Bromo-4-iodonaphthalene Property

Melting point:
88-89℃
Boiling point:
357.3±15.0 °C(Predicted)
Density 
2.057
storage temp. 
2-8°C(protect from light)
form 
Solid
color 
White to Light yellow to Light orange
Water Solubility 
Slightly soluble in water. (3.6 g/L) (25°C)
Sensitive 
Light Sensitive
InChI
InChI=1S/C10H6BrI/c11-9-5-6-10(12)8-4-2-1-3-7(8)9/h1-6H
InChIKey
HQHHKYXPFKHLBF-UHFFFAOYSA-N
SMILES
C1(Br)=C2C(C=CC=C2)=C(I)C=C1
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Safety

HS Code 
2903.99.8001
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4864
Product name
1-Bromo-4-iodonaphthalene
Purity
>98.0%(GC)
Packaging
1g
Price
$73
Updated
2025/07/31
TCI Chemical
Product number
B4864
Product name
1-Bromo-4-iodonaphthalene
Purity
>98.0%(GC)
Packaging
5g
Price
$290
Updated
2025/07/31
TRC
Product number
B686818
Product name
1-Bromo-4-iodonaphthalene
Packaging
30mg
Price
$45
Updated
2021/12/16
TRC
Product number
B686818
Product name
1-Bromo-4-iodonaphthalene
Packaging
60mg
Price
$60
Updated
2021/12/16
TRC
Product number
B686818
Product name
1-Bromo-4-iodonaphthalene
Packaging
300mg
Price
$75
Updated
2021/12/16
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1-Bromo-4-iodonaphthalene Chemical Properties,Usage,Production

Uses

It is used as an OLED material.

Synthesis

2298-07-9

63279-58-3

General procedure for the synthesis of 1-bromo-4-iodonaphthalene from 4-bromo-1-naphthylamine: 1-amino-4-bromonaphthalene (60 g, 0.27 mol) was placed in a single-necked flask and the reaction was carried out under argon protection. Acetonitrile (500 ml) was added as a solvent and the reaction mixture was cooled to 0 °C and kept until 1-amino-4-bromonaphthalene was completely dissolved. Subsequently, boron nitrite (42 g, 49 ml, 0.41 mol) and copper bromide (73 g, 0.32 mol) were added sequentially with continuous stirring for 3 h at room temperature. Upon completion of the reaction, the reaction was terminated by slow addition of 1N HCl aqueous solution (600 ml). The resulting solid product was collected by filtration and washed sequentially with distilled water and ether to remove impurities. Finally, the target compound 1-bromo-4-iodonaphthalene (76 g, 85% yield) was purified by column chromatography.

References

[1] Patent: WO2011/105700, 2011, A1. Location in patent: Page/Page column 23
[2] Patent: US2011/152246, 2011, A1. Location in patent: Page/Page column 121-123
[3] Journal of the Chemical Society, 1885, vol. 47, p. 523
[4] Journal of the Chemical Society, 1895, vol. 67, p. 912
[5] Tetrahedron Letters, 2004, vol. 45, # 42, p. 7883 - 7885

1-Bromo-4-iodonaphthalene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Bromo-4-iodonaphthalene Suppliers

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View Lastest Price from 1-Bromo-4-iodonaphthalene manufacturers

Shenzhen Nexcon Pharmatechs Ltd.
Product
1-Bromo-4-iodonaphthalene 63279-58-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
2000
Release date
2025-04-18
Shanghai Daken Advanced Materials Co.,Ltd
Product
1-Bromo-4-iodonaphthalene 63279-58-3
Price
US $0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
150KG /month
Release date
2021-11-18
Zhuozhou Wenxi import and Export Co., Ltd
Product
1,4-BIN 63279-58-3
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-11

63279-58-3, 1-Bromo-4-iodonaphthaleneRelated Search:

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  • 63279-58-3