ChemicalBook > CAS DataBase List > 4-nitro-6-fluoroindazole

4-nitro-6-fluoroindazole

Product Name
4-nitro-6-fluoroindazole
CAS No.
885520-14-9
Chemical Name
4-nitro-6-fluoroindazole
Synonyms
4-nitro-6-fluoroindazole;6-Fluoro-4-nitro-1H-indazole;1H-indazole, 6-fluoro-4-nitro-
CBNumber
CB72554108
Molecular Formula
C7H4FN3O2
Formula Weight
181.12
MOL File
885520-14-9.mol
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4-nitro-6-fluoroindazole Property

Density 
1.629
storage temp. 
Sealed in dry,Room Temperature
Appearance
Off-white to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B440958
Product name
6-fluoro-4-nitro-1H-indazole
Packaging
10mg
Price
$90
Updated
2021/12/16
AK Scientific
Product number
4340AC
Product name
6-Fluoro-4-nitro-1H-indazole
Packaging
1g
Price
$401
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0048225
Product name
6-FLUORO-4-NITROINDAZOLE
Purity
95.00%
Packaging
5MG
Price
$500.92
Updated
2021/12/16
Alichem
Product number
885520149
Product name
6-Fluoro-4-nitro-1H-indazole
Packaging
1g
Price
$662
Updated
2021/12/16
Crysdot
Product number
CD11032531
Product name
6-Fluoro-4-nitro-1H-indazole
Purity
97%
Packaging
1g
Price
$409
Updated
2021/12/16
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4-nitro-6-fluoroindazole Chemical Properties,Usage,Production

Synthesis

168770-44-3

885520-14-9

5-Fluoro-3-nitro-2-methylaniline (50 mg, 0.294 mmol) was used as starting material and dissolved in acetic acid (AcOH, 10 mL). Aqueous sodium nitrite (3 mL, containing 44.6 mg, 0.588 mmol of sodium nitrite) was slowly added at 0 °C. The reaction mixture was then warmed to room temperature and stirred continuously for 6 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) and the reaction was terminated after confirming the complete consumption of raw materials. The final product 4-nitro-6-fluoroindazole was obtained as 18.3 mg of orange colored powder with 43.5% yield.

References

[1] Patent: CN108689937, 2018, A. Location in patent: Paragraph 0081; 0082; 0087; 0088
[2] Patent: CN108689936, 2018, A. Location in patent: Paragraph 0048; 0054; 0055
[3] Patent: WO2010/127855, 2010, A1. Location in patent: Page/Page column 153; 154
[4] Patent: WO2014/14794, 2014, A2. Location in patent: Page/Page column 80
[5] Patent: WO2008/110863, 2008, A1. Location in patent: Page/Page column 27

4-nitro-6-fluoroindazole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-nitro-6-fluoroindazole manufacturers

Career Henan Chemical Co
Product
4-nitro-6-fluoroindazole 885520-14-9
Price
US $0.01/KG
Min. Order
1KG
Purity
98%; 99%
Supply Ability
500g;1kg; 25kg
Release date
2020-01-09