4-nitro-6-fluoroindazole
- Product Name
- 4-nitro-6-fluoroindazole
- CAS No.
- 885520-14-9
- Chemical Name
- 4-nitro-6-fluoroindazole
- Synonyms
- 4-nitro-6-fluoroindazole;6-Fluoro-4-nitro-1H-indazole;1H-indazole, 6-fluoro-4-nitro-
- CBNumber
- CB72554108
- Molecular Formula
- C7H4FN3O2
- Formula Weight
- 181.12
- MOL File
- 885520-14-9.mol
4-nitro-6-fluoroindazole Property
- Density
- 1.629
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B440958
- Product name
- 6-fluoro-4-nitro-1H-indazole
- Packaging
- 10mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 4340AC
- Product name
- 6-Fluoro-4-nitro-1H-indazole
- Packaging
- 1g
- Price
- $401
- Updated
- 2021/12/16
- Product number
- HCH0048225
- Product name
- 6-FLUORO-4-NITROINDAZOLE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.92
- Updated
- 2021/12/16
- Product number
- A210770
- Product name
- 6-Fluoro-4-nitro-1H-indazole
- Purity
- 97%
- Packaging
- 100mg
- Price
- $62
- Updated
- 2021/12/16
- Product number
- A210770
- Product name
- 6-Fluoro-4-nitro-1H-indazole
- Purity
- 97%
- Packaging
- 250mg
- Price
- $101
- Updated
- 2021/12/16
4-nitro-6-fluoroindazole Chemical Properties,Usage,Production
Synthesis
168770-44-3
885520-14-9
5-Fluoro-3-nitro-2-methylaniline (50 mg, 0.294 mmol) was used as starting material and dissolved in acetic acid (AcOH, 10 mL). Aqueous sodium nitrite (3 mL, containing 44.6 mg, 0.588 mmol of sodium nitrite) was slowly added at 0 °C. The reaction mixture was then warmed to room temperature and stirred continuously for 6 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) and the reaction was terminated after confirming the complete consumption of raw materials. The final product 4-nitro-6-fluoroindazole was obtained as 18.3 mg of orange colored powder with 43.5% yield.
References
[1] Patent: CN108689937, 2018, A. Location in patent: Paragraph 0081; 0082; 0087; 0088
[2] Patent: CN108689936, 2018, A. Location in patent: Paragraph 0048; 0054; 0055
[3] Patent: WO2010/127855, 2010, A1. Location in patent: Page/Page column 153; 154
[4] Patent: WO2014/14794, 2014, A2. Location in patent: Page/Page column 80
[5] Patent: WO2008/110863, 2008, A1. Location in patent: Page/Page column 27
4-nitro-6-fluoroindazole Preparation Products And Raw materials
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View Lastest Price from 4-nitro-6-fluoroindazole manufacturers
- Product
- 4-nitro-6-fluoroindazole 885520-14-9
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 500g;1kg; 25kg
- Release date
- 2020-01-09