ChemicalBook > CAS DataBase List > 4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE

4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE

Product Name
4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE
CAS No.
39861-21-7
Chemical Name
4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE
Synonyms
4-(6-chloro-1h-benzimidazol-2-yl)aniline;4-(5-Chloro-1H-benzo[d]imidazol-2-yl)aniline;4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE;Benzenamine, 4-(6-chloro-1H-benzimidazol-2-yl)-
CBNumber
CB7258972
Molecular Formula
C13H10ClN3
Formula Weight
243.69
MOL File
Mol file
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4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE Property

storage temp. 
2-8°C(protect from light)
Appearance
Light yellow to brown Solid
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
2498AE
Product name
4-(5-Chloro-1H-benzoimidazol-2-yl)-phenylamine
Packaging
1g
Price
$456
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0132341
Product name
4-(5-CHLORO-1H-1,3-BENZODIAZOL-2-YL)ANILINE
Purity
95.00%
Packaging
500MG
Price
$768.08
Updated
2021/12/16
Matrix Scientific
Product number
009837
Product name
4-(5-Chloro-1H-benzoimidazol-2-yl)-phenylamine
Packaging
1g
Price
$378
Updated
2021/12/16
CHESS
Product number
1000369
Product name
AN005017:4-(5-Chloro-1H-benzoimidazol-2-yl)-phenylamine
Purity
96
Packaging
1g
Price
$384
Updated
2021/12/16
Ambeed
Product number
A151962
Product name
4-(5-Chloro-1H-benzo[d]imidazol-2-yl)aniline
Purity
95+%
Packaging
100mg
Price
$50
Updated
2021/12/16
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4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE Chemical Properties,Usage,Production

Synthesis

150-13-0

95-83-0

39861-21-7

General procedure for the synthesis of 4-(5-chloro-1H-benzo[d]imidazol-2-yl)aniline from p-aminobenzoic acid and 4-chloro-1,2-benzenediamine: Eaton's reagent (10% v/v (w/v)) was added drop-wise to a mixture of 4-chloro-1,2-benzenediamine (1 equiv) and p-aminobenzoic acid (1 equiv). Subsequently, the reaction mixture was heated at 130 °C for 5-6 h. The reaction process was monitored by TLC and LCMS. After completion of the reaction, the mixture was cooled to room temperature and neutralized with 10% sodium hydroxide solution to pH 6-7. The precipitate formed was collected by filtration and washed repeatedly with water and subsequently dried. Finally, the resulting solid was purified by ethanol recrystallization to afford the target product 4-(5-chloro-1H-benzo[d]imidazol-2-yl)aniline in good yield.

References

[1] Bioorganic and Medicinal Chemistry, 2014, vol. 22, # 21, p. 5970 - 5987

4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE Suppliers

China 21 Germany 1 India 1 Russia 1 United Kingdom 5 United States 6 Global 35
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
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China
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Shanghai Run-Biotech Co., Ltd.
Tel
021-57171705 13817537615
Fax
QQ3095748324
Email
sales@run-biotech.com
Country
China
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ShangHai AmK Pharmaceutical Technology Co., Ltd.
Tel
微信 17321281695 18019252918
Fax
17321281695
Email
sale@amkchem.com
Country
China
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Yancheng KangdiSen Pharmaceutical Co., Ltd.
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13812573443
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tongbenwan22@163.com
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China
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Amadis Chemical Company Limited
Tel
571-89925085
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0086-571-89925065
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sales@amadischem.com
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China
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Biokitchen
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021-021-021-31663258 13795219287
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021-31663258
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donghuanwen@126.com
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China
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Jiangsu aikang biomedical research and development co., LTD
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025-58859352 13155353615
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qzhang@aikonchem.com
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China
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Shandong Puchuang Pharmaceutical Technology Co., Ltd.
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18953403321
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QQ：2457827970
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3218803372@qq.com
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China
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283
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Zhengzhou Convergence Chemical Co. LTD
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0371-0371-53736046 13393710386
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QQ:2853979814
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2853979814@qq.com
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China
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9947
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Energy Chemical
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021-58432009 400-005-6266
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021-58436166
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marketing1@energy-chemical.com
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China
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44894
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39861-21-7, 4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINERelated Search:


  • 4-(5-CHLORO-1H-BENZOIMIDAZOL-2-YL)-PHENYLAMINE
  • 4-(5-Chloro-1H-benzo[d]imidazol-2-yl)aniline
  • 4-(6-chloro-1h-benzimidazol-2-yl)aniline
  • Benzenamine, 4-(6-chloro-1H-benzimidazol-2-yl)-
  • 39861-21-7
  • C13H10ClN3