3'-BroMo-5'-fluoroacetophenone

Product Name: 3'-BroMo-5'-fluoroacetophenone
CAS No.: 105515-20-6
Chemical Name: 3'-BroMo-5'-fluoroacetophenone
Synonyms: 103541;1-(3-Bromo-5-fL;3'-BroMo-5'-fluoroacetophenone;1-(3-Bromo-5-fluorophnyl)thanon;1-(3-broMo-5-fluorophenyl)ethanone;3'-Bromo-5'-fluoroacetophenone,96%;1-(3-bromo-5-fluorophenyl)ethan-1-one;Ethanone, 1-(3-bromo-5-fluorophenyl)-
CBNumber: CB72594519
Molecular Formula: C8H6BrFO
Formula Weight: 217.04
MOL File: 105515-20-6.mol

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3'-BroMo-5'-fluoroacetophenone Property

Boiling point:: 257.9±25.0 °C(Predicted)
Density: 1.535±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
form: Solid
Appearance: White to yellow Solid

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Safety

HS Code: 2914390090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: B693008
Product name: 1-(3-Bromo-5-fluorophenyl)ethanone
Packaging: 100mg
Price: $70
Updated: 2021/12/16

TRC

Product number: B693008
Product name: 1-(3-Bromo-5-fluorophenyl)ethanone
Packaging: 250mg
Price: $125
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2617-B-89
Product name: 3?-Bromo-5?-fluoroacetophenone
Packaging: 5G
Price: $375
Updated: 2021/12/16

Apolloscientific

Product number: PC501607
Product name: 3’-Bromo-5’-fluoroacetophenone
Packaging: 5g
Price: $316
Updated: 2021/12/16

ChemScene

Product number: CS-0060849
Product name: 1-(3-Bromo-5-fluorophenyl)ethan-1-one
Purity: 99.93%
Packaging: 10g
Price: $238
Updated: 2021/12/16

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3'-BroMo-5'-fluoroacetophenone Chemical Properties,Usage,Production

Synthesis

176548-70-2

105515-20-6

A 1.3 M solution of methyl lithium ether (35 mL) was slowly added dropwise to an ether solution of 3-bromo-5-fluorobenzoic acid (5 g) at -78 °C, maintaining the temperature at -78 °C. The reaction mixture was then slowly warmed to -10 °C and stirred continuously at this temperature for 1 hour. Upon completion of the reaction, the reaction was carefully quenched with saturated ammonium chloride solution (100 mL) until the pH of the reaction system reached 3. The product was extracted with ether (2 x 100 mL), and the combined organic phases were dried over anhydrous sodium sulfate. The solvent was removed by evaporation under reduced pressure to give 1-(3-bromo-5-fluorophenyl)ethanone as an off-white solid (4.67 g, 94% yield). The product was characterized by 1H NMR (CDCl3): δ 2.59 (3H, s, ArCOCH3), 7.44 (1H, dd, Ar), 7.59 (1H, dd, Ar), 7.87 (1H, s, Ar).

References

[1] Patent: US2009/209529, 2009, A1. Location in patent: Page/Page column 35

3'-BroMo-5'-fluoroacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

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3'-BroMo-5'-fluoroacetophenone Suppliers

China 46 India 2 United Kingdom 1 United States 9 Global 58

Alfa Aesar

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105515-20-6, 3'-BroMo-5'-fluoroacetophenoneRelated Search:

3'-BroMo-5'-fluoroacetophenone

1-(3-broMo-5-fluorophenyl)ethanone

103541

1-(3-Bromo-5-fL

Ethanone, 1-(3-bromo-5-fluorophenyl)-

3'-Bromo-5'-fluoroacetophenone,96%

1-(3-bromo-5-fluorophenyl)ethan-1-one

1-(3-Bromo-5-fluorophnyl)thanon

105515-20-6