ChemicalBook > CAS DataBase List > 3'-BroMo-5'-fluoroacetophenone

3'-BroMo-5'-fluoroacetophenone

Product Name
3'-BroMo-5'-fluoroacetophenone
CAS No.
105515-20-6
Chemical Name
3'-BroMo-5'-fluoroacetophenone
Synonyms
103541;1-(3-Bromo-5-fL;3'-BroMo-5'-fluoroacetophenone;1-(3-Bromo-5-fluorophnyl)thanon;1-(3-broMo-5-fluorophenyl)ethanone;3'-Bromo-5'-fluoroacetophenone,96%;1-(3-bromo-5-fluorophenyl)ethan-1-one;Ethanone, 1-(3-bromo-5-fluorophenyl)-
CBNumber
CB72594519
Molecular Formula
C8H6BrFO
Formula Weight
217.04
MOL File
105515-20-6.mol
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3'-BroMo-5'-fluoroacetophenone Property

Boiling point:
257.9±25.0 °C(Predicted)
Density 
1.535±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
form 
Solid
Appearance
White to yellow Solid
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Safety

HS Code 
2914390090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
B693008
Product name
1-(3-Bromo-5-fluorophenyl)ethanone
Packaging
100mg
Price
$70
Updated
2021/12/16
TRC
Product number
B693008
Product name
1-(3-Bromo-5-fluorophenyl)ethanone
Packaging
250mg
Price
$125
Updated
2021/12/16
ChemScene
Product number
CS-0060849
Product name
1-(3-Bromo-5-fluorophenyl)ethan-1-one
Purity
99.93%
Packaging
250mg
Price
$27
Updated
2021/12/16
ChemScene
Product number
CS-0060849
Product name
1-(3-Bromo-5-fluorophenyl)ethan-1-one
Purity
99.93%
Packaging
1g
Price
$38
Updated
2021/12/16
AK Scientific
Product number
Z6809
Product name
1-(3-Bromo-5-fluorophenyl)ethanone
Packaging
100mg
Price
$88
Updated
2021/12/16
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3'-BroMo-5'-fluoroacetophenone Chemical Properties,Usage,Production

Synthesis

176548-70-2

105515-20-6

A 1.3 M solution of methyl lithium ether (35 mL) was slowly added dropwise to an ether solution of 3-bromo-5-fluorobenzoic acid (5 g) at -78 °C, maintaining the temperature at -78 °C. The reaction mixture was then slowly warmed to -10 °C and stirred continuously at this temperature for 1 hour. Upon completion of the reaction, the reaction was carefully quenched with saturated ammonium chloride solution (100 mL) until the pH of the reaction system reached 3. The product was extracted with ether (2 x 100 mL), and the combined organic phases were dried over anhydrous sodium sulfate. The solvent was removed by evaporation under reduced pressure to give 1-(3-bromo-5-fluorophenyl)ethanone as an off-white solid (4.67 g, 94% yield). The product was characterized by 1H NMR (CDCl3): δ 2.59 (3H, s, ArCOCH3), 7.44 (1H, dd, Ar), 7.59 (1H, dd, Ar), 7.87 (1H, s, Ar).

References

[1] Patent: US2009/209529, 2009, A1. Location in patent: Page/Page column 35

3'-BroMo-5'-fluoroacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

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3'-BroMo-5'-fluoroacetophenone Suppliers

China 49 India 2 United Kingdom 1 United States 9 Global 61
Accela ChemBio Inc.
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Accela ChemBio Inc.
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Alchem Pharmtech,Inc.
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Aladdin Scientific
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Synthonix Inc
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Matrix Scientific
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105515-20-6, 3'-BroMo-5'-fluoroacetophenoneRelated Search:


  • 3'-BroMo-5'-fluoroacetophenone
  • 1-(3-broMo-5-fluorophenyl)ethanone
  • 103541
  • 1-(3-Bromo-5-fL
  • Ethanone, 1-(3-bromo-5-fluorophenyl)-
  • 3'-Bromo-5'-fluoroacetophenone,96%
  • 1-(3-bromo-5-fluorophenyl)ethan-1-one
  • 1-(3-Bromo-5-fluorophnyl)thanon
  • 105515-20-6