bis(3-Methoxyphenyl)aMine

Product Name: bis(3-Methoxyphenyl)aMine
CAS No.: 92248-06-1
Chemical Name: bis(3-Methoxyphenyl)aMine
Synonyms: bis(3-Methoxyphenyl)aMine;3-Methoxy-N-(3-methoxyphenyl)aniline;Benzenamine, 3-methoxy-N-(3-methoxyphenyl)-;bis(3-Methoxyphenyl)aMine ISO 9001：2015 REACH
CBNumber: CB72610213
Molecular Formula: C14H15NO2
Formula Weight: 229.27
MOL File: 92248-06-1.mol

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bis(3-Methoxyphenyl)aMine Property

Boiling point:: 175-178 °C(Press: 0.8 Torr)
Density: 1.126±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 0.14±0.50(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H319Causes serious eye irritation
Precautionary statements: P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0391959
Product name: BIS-(3-METHOXYPHENYL)AMINE
Purity: 95.00%
Packaging: 5MG
Price: $505.87
Updated: 2021/12/16

Alichem

Product number: 92248061
Product name: Bis(3-methoxyphenyl)amine
Packaging: 5g
Price: $1085.4
Updated: 2021/12/16

Alichem

Product number: 92248061
Product name: Bis(3-methoxyphenyl)amine
Packaging: 10g
Price: $1407
Updated: 2021/12/16

Alichem

Product number: 92248061
Product name: Bis(3-methoxyphenyl)amine
Packaging: 25g
Price: $2706.8
Updated: 2021/12/16

Ambeed

Product number: A208352
Product name: Bis(3-methoxyphenyl)amine
Purity: 95%
Packaging: 100mg
Price: $21
Updated: 2021/12/16

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bis(3-Methoxyphenyl)aMine Chemical Properties,Usage,Production

Synthesis

10365-98-7

536-90-3

92248-06-1

General procedure for the synthesis of bis(3-methoxyphenyl)amines from 3-methoxyphenylboronic acid and m-aminoanisole: 1. copper acetate (2.1 mmol) and pyridine (0.25 mL) were added to a vigorously stirred solution of anhydrous dichloromethane (3.5 mL) of 3-methoxyaniline (1 mmol) and 3-methoxyphenylboronic acid (2 mmol) under nitrogen protection. 2. The reaction mixture was stirred at room temperature for 72 hours, during which time the progress of the reaction was monitored by thin layer chromatography (TLC). 3. Upon completion of the reaction, the crude reaction mixture was pre-adsorbed onto silica gel and the target product, bis(3-methoxyphenyl)amine (3c), was subsequently isolated by fast column chromatography. 4. Product yield: 25%; EI-MS m/z: 229 (M+) [Ref: Urgaonkar, S.; Verkade, J.G. J. Org. Chem. 2004, 69, 9135-9142].

References

[1] Patent: WO2007/79593, 2007, A1. Location in patent: Page/Page column 31

bis(3-Methoxyphenyl)aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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92248-06-1, bis(3-Methoxyphenyl)aMineRelated Search:

bis(3-Methoxyphenyl)aMine

Benzenamine, 3-methoxy-N-(3-methoxyphenyl)-

3-Methoxy-N-(3-methoxyphenyl)aniline

bis(3-Methoxyphenyl)aMine ISO 9001：2015 REACH

92248-06-1