4-Isopropoxycyclohexanone
- Product Name
- 4-Isopropoxycyclohexanone
- CAS No.
- 69697-46-7
- Chemical Name
- 4-Isopropoxycyclohexanone
- Synonyms
- 4-Isopropoxycyclohexanone;4-isopropoxycyclohexan-1-one;4-(1-Methylethoxy)cyclohexanone;4-(propan-2-yloxy)cyclohexanone;4-propan-2-yloxycyclohexan-1-one;Cyclohexanone,4-(1-Methylethoxy)-
- CBNumber
- CB72614246
- Molecular Formula
- C9H16O2
- Formula Weight
- 156.22
- MOL File
- 69697-46-7.mol
4-Isopropoxycyclohexanone Property
- Boiling point:
- 222℃
- Density
- 0.95±0.1 g/cm3(Predicted)
- Flash point:
- 82℃
- storage temp.
- Sealed in dry,Room Temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H332Harmful if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P322Specific measures (see …on this label).
P330Rinse mouth.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 0776AC
- Product name
- 4-Isopropoxycyclohexanone
- Packaging
- 1g
- Price
- $320
- Updated
- 2021/12/16
- Product number
- CHM0390077
- Product name
- 4-ISOPROPOXYCYCLOHEXANONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.92
- Updated
- 2021/12/16
- Product number
- 116081
- Product name
- 4-Isopropoxycyclohexanone
- Purity
- >90%
- Packaging
- 500mg
- Price
- $544
- Updated
- 2021/12/16
- Product number
- 116081
- Product name
- 4-Isopropoxycyclohexanone
- Purity
- >90%
- Packaging
- 1g
- Price
- $730
- Updated
- 2021/12/16
- Product number
- CM202275
- Product name
- 4-Isopropoxycyclohexanone
- Purity
- 95%
- Packaging
- 5g
- Price
- $1029
- Updated
- 2021/12/16
4-Isopropoxycyclohexanone Chemical Properties,Usage,Production
Synthesis
950771-91-2
69697-46-7
The general procedure for the synthesis of 4-isopropoxycyclohexanone from 8-isopropoxy-1,4-dioxaspiro[4.5]decane was carried out as follows: a tetrahydrofuran solution (10 ml) of 8-isopropoxy-1,4-dioxaspiro[4.5]decane and 4-isopropoxycyclohexanone (approx. 4:1 mixture, D25, 4.89 g, approx. 0.025 mol) was prepared at room temperature and under argon protection ) was treated with 5 M hydrochloric acid (50 ml) and stirred thoroughly for 18 hours. After completion of the reaction, the reaction mixture was diluted with water (150 ml) and extracted with dichloromethane (2 x 80 ml). The organic phases were combined, washed with brine, dried over anhydrous sodium sulfate, and subsequently concentrated under vacuum to give 4-isopropoxycyclohexanone as a colorless oil (3.9 g, 100% yield).1H NMR (CDCl3, 400 MHz) δ: 1.19 (6H, d), 1.88-2.08 (4H, m), 2.22-2.32 (2H, m), 2.54- 2.65 (2H, m), 3.70-3.84 (2H, m).
References
[1] Patent: WO2007/107565, 2007, A1. Location in patent: Page/Page column 61
[2] Patent: WO2007/107566, 2007, A1. Location in patent: Page/Page column 66
[3] Patent: US2011/280808, 2011, A1. Location in patent: Page/Page column 74
[4] Patent: US2015/329529, 2015, A1. Location in patent: Paragraph 0511-0512
4-Isopropoxycyclohexanone Preparation Products And Raw materials
Raw materials
Preparation Products
4-Isopropoxycyclohexanone Suppliers
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- tp@aladdinsci.com
- Country
- United States
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- 52923
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- United States
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- United States
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- admin@intlab.org
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- United States
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View Lastest Price from 4-Isopropoxycyclohexanone manufacturers
- Product
- 4-Isopropoxycyclohexanone 69697-46-7
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2019-12-24