Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
- Product Name
- Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
- CAS No.
- 23428-77-5
- Chemical Name
- Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
- Synonyms
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone;1-(4-methoxy-3-phenylmethoxyphenyl)ethanone;1-(3-(benzyloxy)-4-methoxyphenyl)ethan-1-one;Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]-
- CBNumber
- CB72614680
- Molecular Formula
- C16H16O3
- Formula Weight
- 256.3
- MOL File
- 23428-77-5.mol
Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Property
- Melting point:
- 76 °C
- Boiling point:
- 396.5±27.0 °C(Predicted)
- Density
- 1.115±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Powder
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- Y2092
- Product name
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
- Packaging
- 250mg
- Price
- $158
- Updated
- 2021/12/16
- Product number
- CHM0386724
- Product name
- 1-(3-(BENZYLOXY)-4-METHOXYPHENYL)ETHANONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.21
- Updated
- 2021/12/16
- Product number
- Y2092
- Product name
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
- Packaging
- 5g
- Price
- $1117
- Updated
- 2021/12/16
- Product number
- A121844
- Product name
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $63
- Updated
- 2021/12/16
- Product number
- A121844
- Product name
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $84
- Updated
- 2021/12/16
Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Chemical Properties,Usage,Production
Synthesis
6100-74-9
100-39-0
23428-77-5
In a 200 mL round bottom flask, 4-methoxy-3-hydroxyacetophenone (4.66 g, 28.1 mmol, 1.0 eq.) and potassium carbonate (3.89 g, 28.1 mmol, 1.0 eq.) were added and dissolved in 50 mL of acetone. After stirring for 30 minutes at room temperature, benzyl bromide (5 mL, 29.4 mmol, 1.0 eq.) was slowly added. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the mixture was cooled to room temperature, diluted with 150 mL of pure water, and then extracted with chloroform (100 mL x 4). The organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated. The concentrate was recrystallized with 3 mL of ethyl acetate, filtered and dried under vacuum to obtain the first batch of crystals. The mother liquor was further concentrated, recrystallized with 0.5 mL of ethyl acetate, filtered and dried in vacuum to obtain the second batch of crystals. Coral-like crystals of 1-(3-(benzyloxy)-4-methoxyphenyl)ethanone (compound IV1) were finally obtained, yield: 6.69 g (26.1 mmol, 93% yield).
References
[1] Patent: JP2015/214531, 2015, A. Location in patent: Paragraph 0188; 0189; 0190
[2] Bulletin of the Chemical Society of Japan, 2016, vol. 89, # 1, p. 125 - 134
[3] Beilstein Journal of Organic Chemistry, 2015, vol. 11, p. 884 - 892
[4] Journal of Heterocyclic Chemistry, 2018, vol. 55, # 3, p. 670 - 684
[5] Phytochemistry (Elsevier), 1991, vol. 30, # 7, p. 2438 - 2439
Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Preparation Products And Raw materials
Raw materials
Preparation Products
Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- Suppliers
- Tel
- --
- Fax
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- sales@ajchem.in
- Country
- India
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View Lastest Price from Ethanone, 1-[4-Methoxy-3-(phenylMethoxy)phenyl]- manufacturers
- Product
- 1-(3-(Benzyloxy)-4-methoxyphenyl)ethanone 23428-77-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-10