ChemicalBook > CAS DataBase List > O-[(4-methoxyphenyl)methyl]Hydroxylamine

O-[(4-methoxyphenyl)methyl]Hydroxylamine

Product Name
O-[(4-methoxyphenyl)methyl]Hydroxylamine
CAS No.
21038-22-2
Chemical Name
O-[(4-methoxyphenyl)methyl]Hydroxylamine
Synonyms
HA966-002;HA966-001-2;O-(4-Methoxybenzyl);O-(4-Methoxybenzyl)hydroxylaMine;O-[(4-methoxyphenyl)methyl]Hydroxylamine;Hydroxylamine, O-[(4-methoxyphenyl)methyl]-;O-(4-Methoxybenzyl)hydroxylamine - [M10064];O-[(4-methoxyphenyl)methyl]Hydroxylamine ISO 9001:2015 REACH
CBNumber
CB72623116
Molecular Formula
C8H11NO2
Formula Weight
153.18
MOL File
21038-22-2.mol
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O-[(4-methoxyphenyl)methyl]Hydroxylamine Property

storage temp. 
2-8°C(protect from light)
form 
Solid
color 
White
InChI
InChI=1S/C8H11NO2/c1-10-8-4-2-7(3-5-8)6-11-9/h2-5H,6,9H2,1H3
InChIKey
MVSMBIBGGPSEHQ-UHFFFAOYSA-N
SMILES
NOCC1=CC=C(OC)C=C1
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Synthonix
Product number
M10064
Product name
O-(4-Methoxybenzyl)hydroxylamine
Purity
95+%
Packaging
250mg
Price
$70
Updated
2021/12/16
Synthonix
Product number
M10064
Product name
O-(4-Methoxybenzyl)hydroxylamine
Purity
95+%
Packaging
500mg
Price
$130
Updated
2021/12/16
AK Scientific
Product number
5528AQ
Product name
O-[(4-methoxyphenyl)methyl]hydroxylamine
Packaging
250mg
Price
$152
Updated
2021/12/16
Synthonix
Product number
M10064
Product name
O-(4-Methoxybenzyl)hydroxylamine
Purity
95+%
Packaging
1g
Price
$180
Updated
2021/12/16
Matrix Scientific
Product number
089833
Product name
O-(4-Methoxybenzyl)hydroxylamine
Purity
95+%
Packaging
250mg
Price
$189
Updated
2021/12/16
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O-[(4-methoxyphenyl)methyl]Hydroxylamine Chemical Properties,Usage,Production

Synthesis

2014-61-1

21038-22-2

General procedure for the synthesis of 4-methoxybenzyloxyamine from N-(4-methoxybenzyloxy)phthalimide: To a solution of ethanol (7 mL) containing N-(4-methoxybenzyloxy)phthalimide (0.7 mmol, 236 mg) was added hydrazine hydrate (0.77 mmol, 0.04 mL). The reaction mixture was stirred at 80 °C for 1 hour. After completion of the reaction (monitored by thin layer chromatography), the resulting mixture was concentrated under vacuum. The residue was dissolved in ether, filtered and washed twice with ether. The filtrate was concentrated under vacuum to give 4-methoxybenzyloxyamine as a colorless oil (138 mg, 95% yield).1H NMR (400 MHz, CDCl3) δ 7.31 (d, J = 8.0 Hz, 2H), 6.92 (d, J = 7.9 Hz, 2H), 5.36 (s, 2H), 4.63 (s, 2H), 4.16 (t, J = 4.7 Hz, 2H), 3.60 (t, J = 4.8 Hz, 2H).13C NMR (100 MHz, CDCl3) δ 158.1, 130.2, 130.1, 114.6, 77.5, 67.0, 50.1.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 10, p. 2434 - 2437
[2] Journal of Polymer Science, Part A: Polymer Chemistry, 2010, vol. 48, # 16, p. 3553 - 3563
[3] Molecules, 2013, vol. 18, # 4, p. 3872 - 3893
[4] Bioorganic and Medicinal Chemistry Letters, 2015, vol. 25, # 3, p. 607 - 610
[5] Bioorganic and Medicinal Chemistry Letters, 2003, vol. 13, # 19, p. 3155 - 3159

O-[(4-methoxyphenyl)methyl]Hydroxylamine Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from O-[(4-methoxyphenyl)methyl]Hydroxylamine manufacturers

Career Henan Chemical Co
Product
O-[(4-methoxyphenyl)methyl]Hydroxylamine 21038-22-2
Price
US $1.00/g
Min. Order
1g
Purity
99.0%
Supply Ability
100kg
Release date
2020-01-09

21038-22-2, O-[(4-methoxyphenyl)methyl]HydroxylamineRelated Search:


  • O-(4-Methoxybenzyl)
  • O-[(4-methoxyphenyl)methyl]Hydroxylamine
  • O-(4-Methoxybenzyl)hydroxylaMine
  • HA966-001-2
  • Hydroxylamine, O-[(4-methoxyphenyl)methyl]-
  • HA966-002
  • O-[(4-methoxyphenyl)methyl]Hydroxylamine ISO 9001:2015 REACH
  • O-(4-Methoxybenzyl)hydroxylamine - [M10064]
  • 21038-22-2