ChemicalBook > CAS DataBase List > (6-AMino-5-broMo-pyridin-3-yl)-Methanol
(6-AMino-5-broMo-pyridin-3-yl)-Methanol
- Product Name
- (6-AMino-5-broMo-pyridin-3-yl)-Methanol
- CAS No.
- 1027785-19-8
- Chemical Name
- (6-AMino-5-broMo-pyridin-3-yl)-Methanol
- Synonyms
- 6-AMino-5-broMopyridine-3-Methanol;3-Pyridinemethanol, 6-amino-5-bromo-;(6-AMino-5-broMo-pyridin-3-yl)-Methanol
- CBNumber
- CB72629426
- Molecular Formula
- C6H7BrN2O
- Formula Weight
- 203.04
- MOL File
- 1027785-19-8.mol
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(6-AMino-5-broMo-pyridin-3-yl)-Methanol Property
- Boiling point:
- 344.4±37.0 °C(Predicted)
- Density
- 1.766±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 13.22±0.10(Predicted)
- Appearance
- Light brown to brown Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- A602215
- Product name
- (6-Amino-5-bromopyridin-3-yl)methanol
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
AK Scientific
- Product number
- 3706DT
- Product name
- (6-Amino-5-bromopyridin-3-yl)methanol
- Packaging
- 250mg
- Price
- $174
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 126923
- Product name
- (6-Amino-5-bromopyridin-3-yl)methanol
- Purity
- >95%
- Packaging
- 1g
- Price
- $576
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 126923
- Product name
- (6-Amino-5-bromopyridin-3-yl)methanol
- Purity
- >95%
- Packaging
- 5g
- Price
- $1710
- Updated
- 2021/12/16
Ambeed
- Product number
- A206780
- Product name
- (6-Amino-5-bromopyridin-3-yl)methanol
- Purity
- 97%
- Packaging
- 100mg
- Price
- $58
- Updated
- 2021/12/16
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(6-AMino-5-broMo-pyridin-3-yl)-Methanol Chemical Properties,Usage,Production
Synthesis
850429-51-5
1027785-19-8
General procedure for the synthesis of (6-amino-5-bromopyridin-3-yl)methanol from ethyl 6-amino-5-bromonicotinate: A) Ethyl 6-amino-5-bromonicotinate (2.31 g, 10 mmol) was dissolved in tetrahydrofuran (20 mL) at room temperature and lithium aluminum hydride (LAH, 10 mL, 1 M solution in tetrahydrofuran) was added slowly and dropwise. The reaction mixture was stirred for 1 h. The reaction was quenched by careful addition of water (0.2 mL). The resulting precipitate was collected by filtration and washed with ethyl acetate. The filtrate was concentrated under reduced pressure to give (6-amino-5-bromopyridin-3-yl)methanol (2.0 g, 99% yield) as a white solid. The product was confirmed by LC/MS analysis showing (M + H)+ = 203, 205 (ratio 1:1).1H NMR (CD3OD, 300 MHz) data were as follows: δ 7.79 (s, 1H), 7.67 (s, 1H), 4.35 (br s, 2H).
References
[1] Patent: WO2008/60907, 2008, A2. Location in patent: Page/Page column 34-35
(6-AMino-5-broMo-pyridin-3-yl)-Methanol Preparation Products And Raw materials
Raw materials
Preparation Products
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