4-Metyoxy-2-Methyl-7-azaindole
- Product Name
- 4-Metyoxy-2-Methyl-7-azaindole
- CAS No.
- 307951-52-6
- Chemical Name
- 4-Metyoxy-2-Methyl-7-azaindole
- Synonyms
- 4-Metyoxy-2-Methyl-7-azaindole;4-METHOXY-2-METHYL-1H-PYRROLO[2,3-B]PYRIDINE;1H-Pyrrolo[2,3-b]pyridine, 4-methoxy-2-methyl-
- CBNumber
- CB72656439
- Molecular Formula
- C9H10N2O
- Formula Weight
- 162.19
- MOL File
- 307951-52-6.mol
4-Metyoxy-2-Methyl-7-azaindole Property
- storage temp.
- Sealed in dry,Room Temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 0667CT
- Product name
- 4-Methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine
- Packaging
- 250mg
- Price
- $342
- Updated
- 2021/12/16
- Product number
- A178201
- Product name
- 4-Methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $349
- Updated
- 2021/12/16
- Product number
- CM252093
- Product name
- 4-Methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $729
- Updated
- 2021/12/16
- Product number
- CD11148541
- Product name
- 4-Methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $772
- Updated
- 2021/12/16
- Product number
- 21-2862
- Product name
- 4-methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine
- Purity
- 95%-98%
- Packaging
- 1g
- Price
- $1025
- Updated
- 2021/12/16
4-Metyoxy-2-Methyl-7-azaindole Chemical Properties,Usage,Production
Synthesis
290332-99-9
307951-52-6
General procedure for the synthesis of 4-methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine from 2-methanol-4-methoxy-7-azaindole: (4-methoxy-1H-pyrrolo[2,3-b]pyridin-2-yl) methanol (0.90 g, 5.05 mmol) and Pd(OH)2 (100 mg) were suspended in aqueous solution containing 4N HCl ( 10 mL) in methanol and hydrogenated under hydrogen pressure (50 psi) for 36 hours. Upon completion of the reaction, the acidic mixture was neutralized with 1N NaOH solution. The reaction mixture was filtered through diatomaceous earth, the filtrate was concentrated and purified on a silica gel column using dichloromethane solution containing 5% methanol as eluent to afford the target product 4-methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine (5) as a light yellow slurry. Yield: 0.68 g, 83% yield; ESI MS: m/z 163.01 (M + 1).
References
[1] Patent: WO2007/56184, 2007, A2. Location in patent: Page/Page column 83
[2] Patent: WO2007/56279, 2007, A2. Location in patent: Page/Page column 226; 227
[3] Patent: US2007/135385, 2007, A1. Location in patent: Page/Page column 120-121
4-Metyoxy-2-Methyl-7-azaindole Preparation Products And Raw materials
Raw materials
Preparation Products
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