6-Ethyl-5-iodopyriMidine-2,4-diaMine

Product Name: 6-Ethyl-5-iodopyriMidine-2,4-diaMine
CAS No.: 514854-13-8
Chemical Name: 6-Ethyl-5-iodopyriMidine-2,4-diaMine
Synonyms: 6-Ethyl-5-iodopyriMidine-2,4-diaMine;"2,4-Diamino-6-ethyl-5-iodopyrimidine";2,4-Pyrimidinediamine, 6-ethyl-5-iodo-;6-Ethyl-5-iodopyrimidine-2,4-diamine 97%;2,4-Diamino-6-ethyl-5-iodopyrimidine, 2,4-Diamino-6-ethyl-5-iodo-1,3-diazine
CBNumber: CB72685901
Molecular Formula: C6H9IN4
Formula Weight: 264.07
MOL File: 514854-13-8.mol

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6-Ethyl-5-iodopyriMidine-2,4-diaMine Property

Boiling point:: 431.3±55.0 °C(Predicted)
Density: 1.951±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 6.26±0.10(Predicted)

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

AK Scientific

Product number: 7175AB
Product name: 6-Ethyl-5-iodopyrimidine-2,4-diamine
Packaging: 100mg
Price: $145
Updated: 2021/12/16

Apolloscientific

Product number: OR52066
Product name: 6-Ethyl-5-iodopyrimidine-2,4-diamine
Purity: 97%
Packaging: 250mg
Price: $154
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3730-H-X4
Product name: 6-Ethyl-5-iodopyrimidine-2,4-diamine
Packaging: 250mg
Price: $170
Updated: 2021/12/16

Apolloscientific

Product number: OR52066
Product name: 6-Ethyl-5-iodopyrimidine-2,4-diamine
Purity: 97%
Packaging: 1g
Price: $383
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3730-H-X4
Product name: 6-Ethyl-5-iodopyrimidine-2,4-diamine
Packaging: 1g
Price: $423
Updated: 2021/12/16

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6-Ethyl-5-iodopyriMidine-2,4-diaMine Chemical Properties,Usage,Production

Synthesis

514854-12-7

514854-13-8

General procedure for the synthesis of 6-ethyl-5-iodopyrimidine-2,4-diamine from 2,4-diamino-6-ethylpyrimidine: a suspension of 2,4-diamino-6-ethylpyrimidine (0.8750 g, 5.00 mmol) and iodine monochloride (0.40 mL, 7.50 mmol) was stirred for 2 h at room temperature in methanol (15 mL). Upon completion of the reaction, water (5 mL) was added and the pH was adjusted with 10% NaOH aqueous solution to 7. Subsequently, the reaction mixture was extracted with ethyl acetate (15 mL each time) three times, and the organic phases were combined and dried with anhydrous MgSO4. Finally, the solvent was removed by evaporation to afford the light brown solid product 6-ethyl-5-iodopyrimidine-2,4-diamine (1.1355 g, 86% yield).

References

[1] Patent: WO2017/52479, 2017, A1. Location in patent: Page/Page column 10
[2] Journal of Chemical Research - Part S, 2002, # 10, p. 482 - 484
[3] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 15, p. 3947 - 3963

6-Ethyl-5-iodopyriMidine-2,4-diaMine Preparation Products And Raw materials

Raw materials

Preparation Products

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514854-13-8, 6-Ethyl-5-iodopyriMidine-2,4-diaMineRelated Search:

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514854-13-8