2-(Methylthio)-5-nitropyrimidine-4,6-diol

Product Name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
CAS No.: 1979-97-1
Chemical Name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
Synonyms: 2-(Methylthio)-5-nitropyrimidine-4,6-diol;2-(Methylthio)-5-nitropyrimidine-4,6-diol-2;2-Methylsulfanyl-5-nitro-pyrimidine-4,6-diol;4,6-di hydroxy-2-methyl thio-5-nitro pyrimidine;4(3H)-Pyrimidinone, 6-hydroxy-2-(methylthio)-5-nitro-;4-hydroxy-2-methylsulfanyl-5-nitro-1H-pyrimidin-6-one
CBNumber: CB72693425
Molecular Formula: C5H5N3O4S
Formula Weight: 203.18
MOL File: 1979-97-1.mol

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2-(Methylthio)-5-nitropyrimidine-4,6-diol Property

Melting point:: 223-224 °C
Density: 1.88±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: -0.69±0.10(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M224245
Product name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
Packaging: 50mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: 0186AB
Product name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
Packaging: 250mg
Price: $131
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0388501
Product name: 2-(METHYLTHIO)-5-NITROPYRIMIDINE-4,6-DIOL
Purity: 95.00%
Packaging: 5MG
Price: $496.62
Updated: 2021/12/16

Matrix Scientific

Product number: 100316
Product name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
Purity: 95+%
Packaging: 250mg
Price: $742
Updated: 2021/12/16

Matrix Scientific

Product number: 100316
Product name: 2-(Methylthio)-5-nitropyrimidine-4,6-diol
Purity: 95+%
Packaging: 1g
Price: $1647
Updated: 2021/12/16

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2-(Methylthio)-5-nitropyrimidine-4,6-diol Chemical Properties,Usage,Production

Synthesis

1979-98-2

1979-97-1

Example 99; 4-Hydroxy-4-[3-(trifluoromethyl)phenyl]piperidine-1-carboxylic acid (7-methoxy-5-methylthio-thiazolo[5,4-d]pyrimidin-2-yl)-amide; Step 1: 4,6-dihydroxy-2-methylthio-pyrimidine (10.0 g, 63.22 mmol) was slowly added to fuming nitric acid (30 mL) at 0 °C, the addition process lasted for 1 hour. The reaction mixture was continued to be stirred at 0 °C for 1 h to form a red solution. Subsequently, the reaction solution was poured into ice water and a light brown solid precipitated. The solid was collected by filtration and washed sequentially with water and ether. The resulting solid was dried under vacuum to afford 4,6-dihydroxy-2-methylthio-5-nitropyrimidine (9.30 g, 72% yield) as a light brown solid.LRMS (M+H)+ m/z: 203 (C5H5N3O4S calculated value). The results of nuclear magnetic resonance (NMR) spectral analysis were consistent with the structure of the target compound.

References

[1] Patent: US2007/270433, 2007, A1. Location in patent: Page/Page column 51
[2] Patent: WO2014/9509, 2014, A1. Location in patent: Page/Page column 26; 28
[3] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 6, p. 1658 - 1661
[4] Patent: US2008/4253, 2008, A1. Location in patent: Page/Page column 13
[5] Patent: US2009/156599, 2009, A1. Location in patent: Page/Page column 12

2-(Methylthio)-5-nitropyrimidine-4,6-diol Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(Methylthio)-5-nitropyrimidine-4,6-diol Suppliers

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1979-97-1, 2-(Methylthio)-5-nitropyrimidine-4,6-diolRelated Search:

4-hydroxy-2-methylsulfanyl-5-nitro-1H-pyrimidin-6-one

2-(Methylthio)-5-nitropyrimidine-4,6-diol

2-(Methylthio)-5-nitropyrimidine-4,6-diol-2

2-Methylsulfanyl-5-nitro-pyrimidine-4,6-diol

4(3H)-Pyrimidinone, 6-hydroxy-2-(methylthio)-5-nitro-

4,6-di hydroxy-2-methyl thio-5-nitro pyrimidine

1979-97-1