ChemicalBook > CAS DataBase List > 3-Chloro-5-fluoronitrobenzene
3-Chloro-5-fluoronitrobenzene
- Product Name
- 3-Chloro-5-fluoronitrobenzene
- CAS No.
- 4815-64-9
- Chemical Name
- 3-Chloro-5-fluoronitrobenzene
- Synonyms
- 3-Chloro-5-fluoronitrobenzene;Benzene, 1-chloro-3-fluoro-5-nitro-
- CBNumber
- CB72705764
- Molecular Formula
- C6H3ClFNO2
- Formula Weight
- 175.54
- MOL File
- 4815-64-9.mol
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3-Chloro-5-fluoronitrobenzene Property
- Boiling point:
- 198-200 °C(Press: 762 Torr)
- Density
- 1.494±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
- InChI
- InChI=1S/C6H3ClFNO2/c7-4-1-5(8)3-6(2-4)9(10)11/h1-3H
- InChIKey
- TZAGKOKYKROSOW-UHFFFAOYSA-N
- SMILES
- C1(Cl)=CC([N+]([O-])=O)=CC(F)=C1
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Safety
- HS Code
- 2904990090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- C585063
- Product name
- 1-Chloro-3-fluoro-5-nitrobenzene
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
TRC
- Product number
- C585063
- Product name
- 1-Chloro-3-fluoro-5-nitrobenzene
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
AK Scientific
- Product number
- 5560AQ
- Product name
- 1-chloro-3-fluoro-5-nitrobenzene
- Packaging
- 5g
- Price
- $363.2
- Updated
- 2021/12/16
AK Scientific
- Product number
- 5560AQ
- Product name
- 1-chloro-3-fluoro-5-nitrobenzene
- Packaging
- 250mg
- Price
- $131.6
- Updated
- 2021/12/16
AK Scientific
- Product number
- 5560AQ
- Product name
- 1-chloro-3-fluoro-5-nitrobenzene
- Packaging
- 1g
- Price
- $156.8
- Updated
- 2021/12/16
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3-Chloro-5-fluoronitrobenzene Chemical Properties,Usage,Production
Uses
1-Chloro-3-fluoro-5-nitrobenzene
Synthesis
4863-91-6
4815-64-9
General procedure for the synthesis of 1-chloro-3-fluoro-5-nitrobenzene from 3-chloro-5-fluoroaniline: (a) Sodium perborate tetrahydrate (7.69 g, 50.0 mmol) was suspended in 30 mL of acetic acid and the suspension was heated to 55 °C. 3-Chloro-5-fluoroaniline (1.46 g, 10 mmol) was dissolved in 20 mL of acetic acid and slowly added to the above suspension over a period of 1 hour. The reaction mixture was stirred at 55 °C for 1 h and then cooled to room temperature. To the reaction mixture was added 300 mL of tert-butyl methyl ether (TBME) and the solid was separated by filtration. The organic layer was washed sequentially with saturated saline, 20 mL of aqueous sodium thiosulfate and saturated saline. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to obtain the crude product. The crude product was purified by silica gel column chromatography (40 g SiO?; eluent: cyclohexane) to afford 1-chloro-3-fluoro-5-nitrobenzene as a solid (320 mg, 18% yield). 1H-NMR (400 MHz; DMSO-d6): δ 8.20 (s, 1H), 8.18 (d, 1H), 8.07 (d, 1H).
References
[1] Patent: WO2013/61305, 2013, A1. Location in patent: Page/Page column 46
3-Chloro-5-fluoronitrobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Chloro-5-fluoronitrobenzene manufacturers
Shaanxi Dideu Medichem Co. Ltd
- Product
- 3-Chloro-5-fluoronitrobenzene 4815-64-9
- Price
- US $1.00-1.50/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100000KG
- Release date
- 2024-07-29