Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate

Product Name: Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate
CAS No.: 1316216-05-3
Chemical Name: Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate
Synonyms: Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate;Ethyl 2-(diphenylamino)-5-pyrimidinecarboxylate;5-Pyrimidinecarboxylic acid, 2-(diphenylamino)-, ethyl ester
CBNumber: CB72711961
Molecular Formula: C19H17N3O2
Formula Weight: 319.36
MOL File: 1316216-05-3.mol

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Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate Property

storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: E939093
Product name: Ethyl2-(diphenylamino)pyrimidine-5-carboxylate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: E939093
Product name: Ethyl2-(diphenylamino)pyrimidine-5-carboxylate
Packaging: 50mg
Price: $175
Updated: 2021/12/16

Chemenu

Product number: CM248824
Product name: Ethyl2-(diphenylamino)pyrimidine-5-carboxylate
Purity: 97%
Packaging: 1g
Price: $486
Updated: 2021/12/16

Crysdot

Product number: CD11295359
Product name: Ethyl2-(diphenylamino)pyrimidine-5-carboxylate
Purity: 97%
Packaging: 1g
Price: $515
Updated: 2021/12/16

Chemenu

Product number: CM248824
Product name: Ethyl2-(diphenylamino)pyrimidine-5-carboxylate
Purity: 97%
Packaging: 5g
Price: $1664
Updated: 2021/12/16

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Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate Chemical Properties,Usage,Production

Synthesis

591-50-4

864172-93-0

1316216-05-3

The general procedure for the synthesis of ethyl 2-(diphenylamino)pyrimidine-5-carboxylate from iodobenzene and compound (CAS: 864172-93-0) was as follows: compound 2 (6.2 g, 25 mmol), iodobenzene (6.12 g, 30 mmol), CuI (955 mg, 5.0 mmol), Cs2CO3 (16.3 g, 50 mmol) The mixture in TEOS (200 mL) was degassed and purged with nitrogen. The resulting mixture was stirred and reacted at 140 °C for 14 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was diluted with EtOAc (200 mL) and 95% EtOH (200 mL) and filtered through a pre-prepared column of NH4F-H2O silica gel [50 g, prepared by adding NH4F (100 g) to water (1500 mL) followed by silica gel (500 g, 100-200 mesh)]. The mixture was allowed to stand for 2 h at room temperature before being filtered and the solid was collected and washed with EtOAc. The filtrate was concentrated to dryness and the residue was purified by silica gel column chromatography (petroleum ether/EtOAc = 10:1) to give a yellow solid product (3 g, 38% yield).

References

[1] Patent: WO2011/91213, 2011, A2. Location in patent: Page/Page column 73-74
[2] Patent: WO2013/13113, 2013, A2. Location in patent: Page/Page column 69
[3] Patent: US2015/99744, 2015, A1. Location in patent: Paragraph 0234
[4] Patent: US2015/105384, 2015, A1. Location in patent: Paragraph 0400; 0401
[5] Patent: US2015/105358, 2015, A1. Location in patent: Paragraph 0390-0391

Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate Suppliers

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1316216-05-3, Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylateRelated Search:

ETHYL4-[2-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)ETHOXYL]-3-OXOBUTANOATE ETHYL 4-AMINO-5-IMIDAZOLECARBOXYLATE Isopropenylboronic acid pinacol ester

Ethyl-2-(diphenylaMino)pyriMidine-5-carboxylate

5-Pyrimidinecarboxylic acid, 2-(diphenylamino)-, ethyl ester

Ethyl 2-(diphenylamino)-5-pyrimidinecarboxylate

1316216-05-3