6-BroMoisoquinolin-4-ol

Product Name: 6-BroMoisoquinolin-4-ol
CAS No.: 1015070-56-0
Chemical Name: 6-BroMoisoquinolin-4-ol
Synonyms: 6-BroMoisoquinolin-4-ol;4-Isoquinolinol, 6-bromo-
CBNumber: CB72732595
Molecular Formula: C9H6BrNO
Formula Weight: 224.05
MOL File: 1015070-56-0.mol

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6-BroMoisoquinolin-4-ol Property

Boiling point:: 476.4±25.0 °C(Predicted)
Density: 1.705±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 4.79±0.40(Predicted)
Appearance: Light brown to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0367832
Product name: 6-BROMOISOQUINOLIN-4-OL
Purity: 95.00%
Packaging: 5MG
Price: $504.52
Updated: 2021/12/16

Crysdot

Product number: CD11366814
Product name: 6-Bromoisoquinolin-4-ol
Purity: 95+%
Packaging: 1g
Price: $588
Updated: 2021/12/16

Acrotein

Product number: UT01926
Product name: 6-Bromoisoquinolin-4-ol
Purity: 97%
Packaging: 0.5g
Price: $600
Updated: 2021/12/16

Alichem

Product number: 1015070560
Product name: 6-Bromoisoquinolin-4-ol
Packaging: 1g
Price: $669.5
Updated: 2021/12/16

Chemenu

Product number: CM145038
Product name: 6-bromoisoquinolin-4-ol
Purity: 95%
Packaging: 1g
Price: $729
Updated: 2021/12/16

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6-BroMoisoquinolin-4-ol Chemical Properties,Usage,Production

Synthesis

1235382-79-2

1015070-56-0

General procedure for the synthesis of 6-bromo-4-hydroxyisoquinoline from the compound (CAS: 1235382-79-2): 6-bromo-2-(phenylsulfonyl)-2,3-dihydroisoquinolin-4(1H)-one was first prepared from 4-bromobenzyl bromide with reference to the method reported in Tetrahedron 61 (2005) 8282 (29 g, 79.2 mmol ). The product was then suspended in ethanol (300 mL). To this suspension was added 21% sodium ethoxide/ethanol solution (88.6 mL, 238 mmol) and the reaction was stirred for 1 hour at room temperature. Upon completion of the reaction, 5 M hydrochloric acid (~50 mL) was added to the reaction solution for neutralization, followed by removal of ethanol by distillation under reduced pressure. The precipitated solid precipitate was collected by filtration. The resulting solid was dried and purified by silica gel column chromatography (eluent: dichloromethane/methanol, gradient from 100:0 to 50:50, v/v), resulting in the target product 6-bromo-4-hydroxyisoquinoline (13.2 g, 75% yield).1H-NMR (DMSO-d6) δ: 7.79 (1H, dd, J = 8.7, 1.8 Hz),. 8.03 (1H, d, J = 8.7 Hz), 8.11 (1H, s), 8.25-8.27 (1H, m), 8.82 (1H, s), 10.62 (1H, s).

References

[1] Patent: EP2380878, 2011, A1. Location in patent: Page/Page column 30

6-BroMoisoquinolin-4-ol Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BroMoisoquinolin-4-ol Suppliers

China 20 India 1 United States 3 Global 24

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1015070-56-0, 6-BroMoisoquinolin-4-olRelated Search:

6-BroMoisoquinolin-4-ol

4-Isoquinolinol, 6-bromo-

1015070-56-0