ChemicalBook > CAS DataBase List > 6-BroMo-N1-Methylbenzene-1,2-diaMine
6-BroMo-N1-Methylbenzene-1,2-diaMine
- Product Name
- 6-BroMo-N1-Methylbenzene-1,2-diaMine
- CAS No.
- 1150102-47-8
- Chemical Name
- 6-BroMo-N1-Methylbenzene-1,2-diaMine
- Synonyms
- 6-Bromo-N1-methylbenzene-1,2-diamin;6-Bromo-N1-methyl-1,2-benzenediamine;3-bromo-N2-methyl-1,2-benzenediamine;6-BroMo-N1-Methylbenzene-1,2-diaMine;3-bromo-2-N-methylbenzene-1,2-diamine;1,2-Benzenediamine, 3-bromo-N2-methyl-;3-Bromo-N*2*-methyl-benzene-1,2-diamine
- CBNumber
- CB72735879
- Molecular Formula
- C7H9BrN2
- Formula Weight
- 201.06
- MOL File
- 1150102-47-8.mol
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6-BroMo-N1-Methylbenzene-1,2-diaMine Property
- Boiling point:
- 297.9±30.0 °C(Predicted)
- Density
- 1.578±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 5.48±0.11(Predicted)
- InChI
- InChI=1S/C7H9BrN2/c1-10-7-5(8)3-2-4-6(7)9/h2-4,10H,9H2,1H3
- InChIKey
- BVQOQXXITQULGQ-UHFFFAOYSA-N
- SMILES
- C1(N)=CC=CC(Br)=C1NC
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- B111530
- Product name
- 6-Bromo-N1-methylbenzene-1,2-diamine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0116339
- Product name
- 6-Bromo-N1-methylbenzene-1,2-diamine
- Purity
- 96.03%
- Packaging
- 5g
- Price
- $847
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0116339
- Product name
- 6-Bromo-N1-methylbenzene-1,2-diamine
- Purity
- 96.03%
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0116339
- Product name
- 6-Bromo-N1-methylbenzene-1,2-diamine
- Purity
- 96.03%
- Packaging
- 1g
- Price
- $227
- Updated
- 2021/12/16
Ambeed
- Product number
- A207266
- Product name
- 6-Bromo-N1-methylbenzene-1,2-diamine
- Purity
- 97%
- Packaging
- 1g
- Price
- $235
- Updated
- 2021/12/16
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6-BroMo-N1-Methylbenzene-1,2-diaMine Chemical Properties,Usage,Production
Synthesis
1004618-77-2
1150102-47-8
General procedure for the synthesis of 6-bromo-N1-methylbenzene-1,2-diamine from 2-bromo-N-methyl-6-nitroaniline: a mixture of the product of the previous step, 2-bromo-N-methyl-6-nitroaniline (8 g, 34.62 mmol, 1.00 eq.), with zinc powder (4 g, 62.50 mmol, 2.00 eq.) in acetic acid (120 mL) was reacted at room temperature The reaction was stirred for 16 hours at room temperature. After completion of the reaction, the insoluble solids were removed by filtration and the filtrate was concentrated under vacuum. The concentrated residue was dissolved in dichloromethane (300 mL), washed with saturated sodium bicarbonate solution (100 mL), and the organic phase was dried with anhydrous sodium sulfate and concentrated again under vacuum to give the target product 6-bromo-N1-methylbenzene-1,2-diamine (4 g, 57% yield) as a black oil.LC-MS (electrospray ionization, m/z): 201.
References
[1] Patent: US2018/162822, 2018, A1. Location in patent: Paragraph 0557
[2] Patent: WO2009/58728, 2009, A1. Location in patent: Page/Page column 73
[3] Patent: WO2008/12623, 2008, A1. Location in patent: Page/Page column 62
[4] Patent: WO2017/223229, 2017, A1. Location in patent: Paragraph 00515; 00516
6-BroMo-N1-Methylbenzene-1,2-diaMine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-BroMo-N1-Methylbenzene-1,2-diaMine manufacturers
Shaanxi Dideu New Materials Co. Ltd
- Product
- 6-BroMo-N1-Methylbenzene-1,2-diaMine 1150102-47-8
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1000kg
- Release date
- 2025-05-16