1,4-Diazabicyclo[3.2.1]octane
- Product Name
- 1,4-Diazabicyclo[3.2.1]octane
- CAS No.
- 5167-08-8
- Chemical Name
- 1,4-Diazabicyclo[3.2.1]octane
- Synonyms
- 1,4-Diazabicyclo[3.2.1]octane
- CBNumber
- CB73043335
- Molecular Formula
- C6H12N2
- Formula Weight
- 112.17
- MOL File
- 5167-08-8.mol
N-Bromosuccinimide Price
- Product number
- 3H31-1-8G
- Product name
- 1,4-Diazabicyclo[3.2.1]octane
- Packaging
- 250mg
- Price
- $508
- Updated
- 2021/12/16
- Product number
- CCH0004054
- Product name
- 1,4-DIAZABICYCLO[3.2.1]OCTANE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $2032.8
- Updated
- 2021/12/16
- Product number
- CM335923
- Product name
- 1,4-Diazabicyclo[3.2.1]octane
- Purity
- 95%+
- Packaging
- 100mg
- Price
- $188
- Updated
- 2021/12/16
- Product number
- CM335923
- Product name
- 1,4-Diazabicyclo[3.2.1]octane
- Purity
- 95%+
- Packaging
- 250mg
- Price
- $336
- Updated
- 2021/12/16
- Product number
- CM335923
- Product name
- 1,4-Diazabicyclo[3.2.1]octane
- Purity
- 95%+
- Packaging
- 1g
- Price
- $669
- Updated
- 2021/12/16
1,4-Diazabicyclo[3.2.1]octane Chemical Properties,Usage,Production
Synthesis
To a slowly stirring
suspension of 11.6 g of 13 (0.0523 mol) in 8.7 mL of H2O was added
a solution of 8.7 g (0.378 mol) of NaOH in 8.7 mL of H2O, which effected almost complete solution. The resulting solution was
extracted three times with CHCl3; the combined extracts were
dried with Na2SO4, filtered, and evaporated to give 5.68 g of yellow
oil. This was treated with excess concentrated HCl and evaporated
to dryness. The semisolid was triturated in acetone and EtOH,
quickly filtered, and dried under N2 to yield 6.75 g (70%) dihydrochloride salt, mp 340 ℃ dec (lit.16 mp 348 ℃ dec).[1]
References
[1] PRISCILLA A. STURM. Antifilarial agents. 3-Aminopyrrolidine and 1,4-diazabicyclo[3.2.1]octane derivatives as analogs of diethylcarbamazine[J]. Journal of Medicinal Chemistry, 1977, 20 10: 1333-1337. DOI:10.1021/jm00220a021.
1,4-Diazabicyclo[3.2.1]octane Preparation Products And Raw materials
Raw materials
Preparation Products
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